LABORATORY HYDROTREATING-REFORMING UNIT

Specialized wavelength-dispersive XRF analyzer based on the Cochois scheme is designed for high-precision determination of chemical elements U, Th, Mo, Au, W, Tl, As, Pb as well as other elements in ores, rocks and when developing the technogenic fields. Possibility to determine groups of elements without readjustment of crystal-analyzer. Exceptionally high resolution of the Koshua X-ray optical scheme with crystal-analyzer quartz 1011. Developed mathematical support. Principle of analyzer operation is based on the excitation of the fluorescent radiation of sample atoms being under examination by radiation coming from an X-ray tube. Spectrum decomposition of the fluorescence radiation is performed according to Cauchois method. The fluorescence radiation focused by analyzing crystal and standard line are marked on Rowland focal circle. Then, they are recorded by X-ray radiation detector in turn. The intensity of the fluorescent irradiation with a particular wavelength is directly proportional to the chemical element concentration in the material under examination.

The chemical-resistant diaphragm pump PL.HM03.01.45 is designed for a wide range of industrial and laboratory tasks, mainly related to pumping vapors/gases. The pumping speed is 38 l/min with a maximum residual pressure of 45 mbar. The device has fairly compact dimensions. Operates from a standard 220 V power supply. Does not require special preparation before use. Post-warranty and warranty service is available throughout the Russian Federation. Characteristics Valve(s) material Standard: chloroprene copolymer NO-68-1 (TU 38 0051166-98) A country Russia Power, W 180 Overall dimensions, L×W×H, mm 289x140x200 Protection class acc. to DIN EN60529 IP20 Noise level, dB no more than 75 Nutrition 220 V/50 Hz Ultimate vacuum, mbar abs. 45 Excess pressure, bar. maximum allowable 0.5 Productivity, l/min 38 Fitting, inch (mm) External diameter, 9 mm. Maximum current, A 1.2 Device weight, kg 7.6 Working chamber material PTFE (polytetrafluoroethylene) Equipment Vacuum pump, cable, instructions, passport, packaging (vacuum regulator and spare parts are not included in the kit and must be ordered separately).

The analyzer is designed to determine the mass fraction of sulfur in automotive fuel in accordance with GOST R 52660-2006 / GOST ISO 20884-2016, ASTM D6334, as well as in oil and petroleum products according to GOST R 53203-2008 / GOST 33194-2014, ASTM D2622, GB/T 11140-2008. Depending on the customer's needs, the analyzer is configured to work in accordance with a particular standard. Implements an arbitration method for measuring the mass fraction of sulfur in automobile fuel of the third, fourth and fifth classes. The device is designed specifically for high-quality and fast X-ray fluorescence analysis of fuel in accordance with the technical regulations "On requirements for automotive and aviation gasoline, diesel and marine fuel, jet fuel and heating oil", which establishes an arbitration X-ray fluorescence wave dispersion method for determining the mass fraction of sulfur in automotive fuels of the third, fourth and fifth classes. The wave dispersion sulfur analyzer SPECTROSCAN SW-D3 is designed taking into account all the requirements for the process of X-ray fluorescence elemental analysis of low sulfur contents in petroleum products. The operator's actions when performing measurements are minimized: - the number/name of the sample is entered from the built-in keyboard; - the sample is poured into two cuvettes; - the obtained samples are placed in the analyzer and measurements are started. The analyzer performs all subsequent actions automatically without operator involvement: - calculates and displays the sulfur content in the sample; - calculates convergence - the difference in determining the mass fraction of sulfur in the first and second samples; - prints measurement results on the built-in printer.

The analyzer allows you to determine the content of sulfur and nitrogen in oil and petroleum products (diesel fuel, gasoline, kerosene, gas oil and any distillate petroleum products), hydrocarbon gas, liquefied petroleum gas (LPG), natural gas, liquefied natural gas (LNG), chemical synthesis products, biological materials by ultraviolet fluorescence and chemiluminescence. The analyzer is a proprietary development of NPO "SPEKTRON". The device is manufactured in St. Petersburg mainly from domestic components. There is a conclusion of the Ministry of Industry and Trade on the production of products in the territory of the Russian Federation. The analyzer is designed to determine: - mass fraction of sulfur in accordance with GOST ISO 20846-2016, GOST 34712-2021, GOST R 56866-2016, GOST 34237-2017, ASTM D5453-19, ASTM D6667-21, ASTM D7551-15, ISO 20729-17 ; - the mass fraction of nitrogen in accordance with ASTM D4629-17. A wide range of concentrations: from ultra-low to high. Modular principle: Each detector is a separate module. The device is equipped individually for each specific task. The possibility of simultaneous determination of sulfur and nitrogen in the analysis process. The principle of operation of the analyzer is to burn the test sample in an oxygen-enriched atmosphere or air at a temperature of 1050 ° C. The sulfur dioxide (SO2) and nitrogen oxide (NO) formed during combustion are transferred by carrier gas to the detection units with preliminary removal of water vapor, on the desiccant, and soot, on the filter. Determination of sulfur is carried out by ultraviolet fluorescence. Determination of nitrogen by chemiluminescence.

It is designed for recording absorption spectra of solid, liquid and gaseous substances in the near and middle IR region (including drugs, lacquers and paints, petroleum products, explosives, pharmacological preparations, polymer films and fibers) with their subsequent identification, as well as for qualitative and quantitative analysis of mixtures containing several components.

High-pressure syringe pump (NSHVD-1) with a continuous highly stable fluid flow in a wide flow range of 0.01-10ml/min. with the functions of introducing a correction factor after calibration, setting the volume or pumping time, displaying the amount of pumped, temporary suspension of pumping with automatic resumption, the ability to adjust the flow and volume of the pumped liquid during operation without stops, automatic shut-off of the pump when the set maximum pressure is exceeded, remote control, compensation for changes in the mass flow rate of the liquid pumped by the pump when its temperature changes. TECHNICAL CHARACTERISTICS Flow range, ml/min 0.01 - 10 Dosing error, % 0.2 The discreteness of the task, % 0.01 Maximum working pressure, 12 bar Lifting height of the suction fluid, m2 Accuracy of pressure measurement, % 0.2 The maximum liquid temperature is 60 °C Modbus RTU communication interface Power supply AC 220 V, 50 Hz Dimensions: W x D x H, mm 140 x 335 x 270 Materials in contact with the pumped liquid glass, fluoroplast, stainless steel 316 L

It is used in technological processes of nuclear, thermal and electric power plants, boiler houses and other facilities for cooling samples supplied to automatic and manual chemical control devices.Easy-to-clean collapsible structure. Materials with high mechanical properties are used: the coil is made of 316 SS steel, the body is made of 304 steel (or 12X18H10T). It is equipped with crimp fittings for connecting sample lines without welding. It is equipped with a special three-way ball valve for supplying / draining cooling water and a control valve that provides a change in the flow of cooling water through the heat exchanger.

The characteristics of the device are similar to the GVCH-12D model; the difference is in the absence of a reactor to remove traces of oxygen and the capacity, respectively, is 25 liters/hour (416 ml/min). Technical specifications Purity of hydrogen in terms of dry gas about 99.998% The concentration of water vapor at 20 OC and 1atm is not more than 10 ppm In the output pressure stabilization mode The range of the specified output pressure of hydrogen is from 1.5 to 6.1 ati Stability of the output pressure of hydrogen is not worse ± 0.02 ati Maximum hydrogen capacity, reduced to normal conditions is 25 l/h The time of setting the operating mode, with the output turned off is no more than 20 minutes In the performance stabilization mode: The range of the specified hydrogen performance is from 0 to 25 l/h Maximum developed pressure in performance mode is 5.0 ati Volume of distilled water to be poured is 1.0 l Distilled water consumption is not more than 0.04 l/hour Water consumption is 2.4 g/l of hydrogen The average life of a replaceable deionization filter cartridge (at maximum performance and single-shift operation) is at least 0.5 years Average power consumption: in stationary mode is no more than 200 VA maximum (at startup) is no more than 250 VA Overall dimensions of the generator, (width x depth x height) are not more than 230x470x450 mm The mass of the generator is not more than 16 kg Operating conditions: ambient temperature, °C, from +10 to +35 powered by single-phase AC voltage, V, 220 (+10 -15)% and frequency, Hz, 50 +1 The generator for electrical safety meets the requirements of Class 1, type H according to GOST 12.2.025-76

Technical specifications: Method of ionization Plasma pulsed glow discharge Discharge gas Argon, consumption less than 1 l/hour Time-of-flight Mass Analyzer with mesh-free ion mirror Resolution 4000 The number of simultaneously defined components is unlimited Mass range 1-1000 m/z Detection limits 1-100 ppb Layer-by-layer resolution Up to 5 nm Depth of analysis Up to 30 microns The time for one analysis of a solid sample is 30 minutes (with the option of a revolver system – 3-5 minutes) Vacuum system 1 Booster pump and 2 TMN (240 l/sec) Overall dimensions 1450×780×1550 mm

The XRF analyzer BRA-135F is an energy dispersive spectrometer which can simultaneously determine the presence of up to twenty chemical elements - from 9F to 92U - in the analyzed sample. Samples can be in liquid, solid, powdered or deposited on a substrate. The analyzer captures concentrations from tenths of mg/kg. The model BRA-135F performs quantitative/semi-quantitative spectral analysis of steel and alloys. It also performs spectral analysis of oil, petroleum and other petroleum products, detecting in their composition even the smallest concentrations of impurities of various metals. The vacuum sample chamber and ultra-slim detector inlet provides a low detection limit in the range of light elements from 9F to 17Cl. The high-performance silicon drift detector (SDD) with an energy resolution of less than 135eV allows the separation of spectral lines of almost all elements, which makes the analysis of complex multicomponent substances (high-alloy steels, precision alloys, polymetallic ores, etc.) possible.

The characteristics of the device are similar to the GVCH-12A model. The difference is the generator capacity of 16 liters /hour. Technical specifications Purity of hydrogen in terms of dry gas is about 99.9999% Concentration of water vapor at 20OC and 1atm is not more than 5 ppm Total hydrogen capacity, reduced to normal conditions is not less than 16 l/h The range of the specified output pressure of hydrogen is from 3.0 to 6.1 ati Stability of the output pressure of hydrogen is not worse than ± 0.02 ati The time of setting the operating mode, with the output turned off is no more than 30 min Volume of distilled water to be poured is 1.0 l Distilled water consumption is no more than 0.03 l/hour Water consumption is 1.6 g/l of hydrogen The average life of the replaceable cartridge of the deionization filter (at maximum performance and single-shift operation) is not less than 1 year Average power consumption: in stationary mode is no more than 220 VA maximum (at startup) is no more than 250 VA Overall dimensions of the generator, (width x depth x height) are not more than 230x470x450 mm The mass of the generator is not more than 17 kg Operating conditions: ambient temperature is from +10 to +35 °C powered by single-phase AC voltage, V, 220 (+10 -15)% and frequency, Hz, 50 +1 The generator for electrical safety meets the requirements of Class 1, type H according to GOST 12.2.025-76

The latest development, the Primelab high-power top-drive mixer, has virtually no analogues even among models from the world's leading manufacturers. It helps solve a wide range of problems related to mixing dense, viscous samples, reagents, and materials. With its help, you can achieve rapid homogenization of the mixture. A significant plus: the graphic display is large and easy to read. With it, the employee working with the mixer will not get tired eyes, even if the mixing work needs to be carried out for several hours in a row. The steel case with durable plastic inserts is resistant to damage, which provides good protection for the device mechanism. The model is easy to operate. It works quite quietly and does not produce a lot of splashes. Main applications of the mixer: • light industry; • petrochemistry; • pharmaceuticals; • medicine; • physical and chemical analysis. Features and Benefits • Thanks to the ergonomic design of the stirrer body, it can be used not only in stationary laboratories, but also in mobile mobile stations. • The submersible type device is used to implement a wide range of laboratory work. • Starting and stopping the mixer is carried out using just one button located on the front panel. • Smooth power control handle. • The noise level remains no more than 50 dB, which creates comfortable working conditions for employees with this equipment. • An overheating system is provided, which is ensured by design features. Characteristics • Country Russia • Display type: LCD • Stirrer shaft diameter max.: 10 mm • Motor type: Brushless • Voltage: 220/50 V • Protection class acc. with DIN EN60529: IP42 • Sample volume (water): 50 liters • Timer: yes (digital) • Device weight: 2.8 kg • Dimensions, WxHxD: 72x260x197 (without rod) • Power consumption, W: 105 • Grounding: Yes • Overheat protection (shutdown): Yes • Maximum torque: 1.3 Nm (at 360 rpm) • Rated torque: 0.4 Nm (at 2200 rpm) • Rotation speed: 20-3000 rpm • Speed adjustment: Encoder (Valcoder) • Accuracy of maintaining the set speed: 5% • Limit state signaling: Optical and acoustic • Display color: Color • Resolution of rotation speed setting: 1 rpm • Chuck type: Three-jaw with manual locking • Parameter display: Optical • Resolution of rotation speed display: 1 rpm • Display size (diagonal, inches): 2.4 Contents: The device delivery set includes: 1) device – 1 pc.; 2) power supply – 1 pc.; 3) power cable – 1 pc.; 4) instruction manual combined with a passport – 1 pc.; 5) bracket Ø13 mm. for attaching the device to a tripod – 1 pc.; 6) hex key 2 mm. - 1 PC.

The ASE-2 energy dispersive sulfur analyzer is designed to measure the mass fraction of sulfur in unleaded gasoline, diesel fuel, crude oil, kerosene, oil residues, lubricating oil bases, hydraulic oils, jet fuels and other distillate oil products. X-ray radiation from a low-power X-ray tube, converted by a primary radiation filter, excites fluorescence emission from the atoms of the sample being analyzed. The fluxes (primary X-rays scattered on the sample and secondary fluorescence) of radiation fall on a gas proportional counter, whereby the fluorescence radiation of sulfur atoms (SKa) is separated from the radiation with other energies by means of selective filters. The intensity of the fluorescence emission of sulfur atoms registered by the gas proportional counter is proportional to the mass fraction of sulfur in the analyzed sample.

The liquid chromatograph "Lumachrom-M" provides maximum automation of the analysis. The device is controlled using specialized software, which in combination with the continuous eluent supply mode and the autosampler gives the maximum level of autonomy of operation. In addition, such a solution minimizes labor costs and the influence of the human factor. The unique design solutions of the chromatograph provide continuous pulsation-free flow of the mobile phase in both isocratic and gradient modes, as well as the ability to work with any column sizes. Thanks to the improved technical characteristics on the Lumachrom-M device, it is possible to implement a wider list of techniques and GOST compared to previous models.

A membrane nitrogen station is a set of equipment for the production and supply of nitrogen under high pressure obtained from atmospheric air by the method of membrane separation. Unlike the membrane nitrogen plant, the membrane nitrogen station is equipped with additional equipment: a booster compressor that creates the necessary pressure. Put the squeeze on the pump. Composition of a typical membrane nitrogen station: 1. Air compressor 2. Dehumidifier 3. Main filter block, including coal column 4. Air receiver 5. Membrane nitrogen generator 6. Nitrogen receiver 7. Nitrogen booster compressor putting the squeeze on

The characteristics of the device are similar to the GCHA-18-K model. The difference is the generator capacity of 15 liters /hour. An oil-free compressor is also built into the generator, which ensures complete autonomy of the device. The warranty for the device is 18 months, for the built–in compressor - 12 months from the date of sale. Technical specifications The grade of nitrogen produced according to GOST 9293-74 is high purity, grade I The volume fraction of nitrogen is not less than, % by volume (including impurities of inert gases — argon, neon, helium) 99.999 The volume fraction of oxygen is not more than, % vol. (ppm) 0.0005 (5 ppm) The volume fraction of water vapor is not more than, % vol. (ppm) 0.0007 (7 ppm) The volume fraction of hydrogen is not more than, % vol. (ppm) 0.0002 (2 ppm) The volume fraction of the sum of carbon-containing compounds in terms of methane is not more than, % vol. (ppm) (with a methane content in the supply air of not more than 4 ppm) 0.0003 (3 ppm) The maximum volume of nitrogen production is not less than 15 liters/hour (250 ml/min) Nominal output pressure of nitrogen is 4 ati The time of setting the operating mode for single-shift operation is no more than, min,* 45 Noise level generated by the compressor is no more than 45 dB Power consumption is not more than 200 VA Overall dimensions, (width x depth x height), not more than, mm, 230x470x510 Weight, not more than, kg 23 Working conditions: ambient temperature, C°, from +10 to +35 Electric power supply from single-phase AC mains voltage, V, 220± 10% and frequency, Hz, 50 ± 1 Average full service life are at least 6 years The generator for electrical safety meets the requirements of Class 1, type H according to GOST 12.2.025-76