CR-1B Reactor by Tetraquant

An automated installation for determining the wear of various catalysts, including KPS (FCC) for cracking with a fluidized bed by an air jet and is designed to determine the comparative wear characteristics of the KPS (FCC) of the catalyst by friction of an air jet according to ASTM D5757-11. It is used for testing with irregularly shaped spherical sludge particles (size from 10 to 180 microns). Abrasion is achieved by fluidization of the sample under the influence of jets of moist air. The percentage of fine particles (less than 20 microns in size) after a 5-hour test is an air jet abrasion index (AJI). technical specifications The range of operating air pressures for the power supply of the installation is 0.8±0.1 MPa The range of air flow rates for the power supply of the installation is not less than (l/min) 20 Absolute error of the air flow rate maintained automatically at a flow rate of 10 l/min. no more, l/min. ± 0.05 Power consumption not more than 0.2 kW Overall dimensions, mm and weight kg. 560x760x1700, 30 Abrasion pipe made of steel 12x18 n10t with dimensions, mm 710±10, 35 ± 0.5 Three sapphire nozzles with a diameter and length, mm 0.381±0.005, 2±1.0 Continuous operation mode Control: microprocessor with tactile control for setting the display and automatic maintenance of installation parameters and mathematical processing of analysis results 60 The convergence of the results when testing the same catalyst is not more than 0.1%

All glass components are made of 3.3 borosilicate glass, which is highly durable, and the frame is made of durable stainless steel. Suitable for working with flammable reagents. The entire apparatus is mounted on a movable frame with wheels for easy movement. The main part is the reaction flask, the volume of which is 100 liters. The package also includes a 30-liter jacket, a control unit with digital display of parameters, a lid with six holes, a dropping funnel, a top-drive stirrer with a motor, and a refrigerator with a receiving flask. At the bottom of the reaction boiler there is a drain valve for unloading the finished product.

The bench laboratory unit is designed to test the adsorption properties of silica gels, protective layers and selective hydrogenation catalysts. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Power supply – three- or single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz.; air 0.4 — 0.8 Mpa. The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS Operating pressure range, MPa 0÷6 Reactor operating temperature range, 0C 20÷600 Reactor inner diameter, mm 20 Internal length of the reactor, mm 690 A thermocouple pocket with a movable filter and a support grid fixed on it to regulate the volume of the tested catalyst. Length of the isothermal zone, mm 300 The type of furnace is Casement Number of thermostatically controlled independent zones 4 The power consumed by each of the four independent thermostatic zones, W ≤ 400 The discreteness of the temperature setting, 0C 0.1 Flow range C2 H4, l/min 0,02÷1,7 Flow range C3 H6, l/min 0,02÷1,7 Flow range H2, l/min 0÷0.02 Flow range N2, ml/min 0.02÷1.7 Actuation pressure of mechanical safety valves, 6,8 MPa Supply voltage 220V 50Hz Power consumption not more than, kW 5 The discreteness of the temperatures and flow rates displayed on the displays is 0.01 Installation weight, kg 230 Overall dimensions of the installation, mm 1680x1480x580 Length of supply gas pipelines, m 20

The glass reactor RGPF II from Primelab is a laboratory device of a non-standard shape. The design contains several sections necessary to create the required conditions in laboratory processes. There are two side outlets, at the ends of which olives are provided for a reliable and durable connection to the equipment using soft hoses. The glass reactor RGPF II is a development of the Primelab company, which produces laboratory glassware and instruments to order according to the customer’s technical specifications. The conditions and terms of production depend on the volume of work.

The unit is designed to determine the so-called Davison index (the ratio of catalyst fractions with a particle size of less than 20 microns before and after analysis), which characterizes the abrasion resistance of microspherical catalysts of the cracking process in a fluidized bed. The installation is included in the register of testing facilities.

Characteristics Maximum heating temperature, °C up to +200 °С Minimum cooling temperature -120 °C Speed range, rpm 60-600 Shaft diameter, mm 12 Nutrition 220 V Heater power, W 4000 (bath heating) Volume, l thirty Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating Engine power, W 90, 3:1 gear motor

Characteristics Minimum cooling temperature -120 °C Speed range, rpm 60-1000 Nutrition 220 V Heater power, W 1500 (bath heating) Volume, l 2 Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating 7 mm Engine power, W 60 Maximum plate heating temperature, °C up to +200 °С

Catalytic reforming is used to produce high-octane components of automobile gasoline, flavored concentrate for the production of individual aromatic hydrocarbons, as well as technical water. Isomerization of paraffin hydrocarbons is used to increase the octane number of C5 - C6 oil fractions by converting paraffins of normal structure into their isomers having a higher octane number.oroda. Hydrotreating of distillates is used to improve the quality and stability of light distillates, raw materials of catalytic cracking, as a result of the use of reactions of destructive hydrogenation of organosulfur compounds and hydrogenation of unsaturated hydrocarbons. Catalytic cracking is used to obtain additional amounts of light petroleum products, namely high-octane gasoline and diesel fuel, by decomposition of heavy oil fractions in the presence of a catalyst. Alkylation of isobutane with olefins is used to produce gasoline fractions with high stability and detonation resistance using the reaction of interaction of isobutane with olefins in the presence of a catalyst. Polymerization (oligomerization) of olefins is used to produce low molecular weight polymers (oligomers) of propylene and butylene used as motor fuel or raw materials for petrochemical synthesis. Hydrocracking is used to obtain an additional amount of light petroleum products by catalytic decomposition of heavy raw materials in the presence of hydrogen. Thermal cracking and Visbreaking is used to obtain in the mode of thermal cracking – additional amounts of light petroleum products by thermal decomposition of residues from oil distillation, in the mode of visbreaking – improving the quality of boiler fuel Coking is used to produce petroleum coke and an additional amount of light petroleum products from heavy residues. The raw materials are tar, thermal cracking residue, heavy gas oil. The products are, for example, petroleum coke.

The reactor has a modular design, so it can be quickly assembled and disassembled. It has a standard package, which includes a 3-liter reaction vessel with a jacket, two valves, a lid with holes for components, a top-drive stirrer with a nozzle, a 60 W asynchronous brushless motor and a dropping funnel. There is a condenser with a vacuum port and an electronic control unit. These parts are assembled onto a mounting rack, which is attached to a massive platform for the stability of the entire reactor. Characteristics Valve(s) material PTFE (Teflon). This is what the seals are made from. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum ≥-0.098 Nutrition 220 V/ 50 Hz Volume, l 3 Mixer power, W 60 Material glass Boro 3.3., photoroplast, steel SS304

Characteristics Valve(s) material PTFE (Teflon). The seals are also made from it. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum 0.098 Nutrition 220 V/ 50 Hz Volume, l 1 Mixer power, W 40 Material Stirrer rod: SS304, PTFE coated blades Housing material and other glass elements - GG17 glass (3.3).

The device consists of the following parts: 200 liter glass flask with jacket; Glass cover with five openings for connecting additional equipment/components; Top drive mixer with anchor; Drip funnel; Condenser with receiving vessel; Control block. All parts are mounted on a steel frame with wheels. Thanks to this, the reactor can be easily moved from one part of the room to another. It has a modular design, easy to assemble and disassemble. All connections are equipped with chemically resistant fluoroplastic gaskets. Glass accessories are made of durable 3.3 borosilicate glass. Characteristics Voltage, V 220 Reaction flask volume, l 200 Material stainless steel, borosilicate glass 3.3 Execution movable steel frame

The 10 liter SF laboratory reactor is a complete medium-sized unit. In terms of functionality, it is not inferior to large production models. It has a modular design and consists of interchangeable parts. Thanks to this, the reactor can be prepared for a specific task. In particular, you can connect a lot of additional equipment to it: various sensors, a thermostat, a vacuum pump, etc. The design of the device is well thought out and easy to use. The reaction vessel is made of borosilicate glass 3.3. It is equipped with a jacket for supplying coolant and a cover with holes for connection with additional equipment. These include a refrigerator, a vacuum valve, a loading funnel, a top-drive stirrer attachment, a temperature sensor, etc. The operation of the stirrer can be controlled using an electronic control unit. The entire structure is mounted on a steel frame with wheels, and the parts are interconnected with Teflon seals. Characteristics Valve(s) material PTFE discharge valve Speed range, rpm 60-1000 Shaft diameter, mm 12 Volume, l 10 Mixer power, W 90 W, 3:1 gear motor Vacuum, MPa 0.098 Material Stirrer rod: SS304, PTFE coated blades Housing material and other glass elements - Boro glass (3.3). Dimensions in packaging 100x58x66 cm, 70 kg

Technical specifications: Operating temperature range, °C 50 ... 175 The discreteness of the temperature setting, °C 0.1 Temperature setting accuracy, °C ± 2 Accuracy of temperature maintenance, °C ± 0.5 Time interval setting range from 1 min to 20 h 59 min Time setting discreteness, min 1 Power consumption, V * A, no more than 450 The size of the landing nest (diameter x depth), mm 17 x 72 Number of landing nests, pcs 29 Overall dimensions, mm, not more than 300 x 300 x 120 Weight, kg, not more than 8

Characteristics Minimum cooling temperature -120 °C Speed range, rpm 60-600 Nutrition 220 V Heater power, W 2000 (bath heating) Volume, l 10 Vacuum, MPa 0.098 Material stirrer head: stainless steel coated with PTFE 12 mm Engine power, W 90, 3:1 gear motor Maximum plate heating temperature, °C up to +200 °С

The reactor has a modular design, making it easy to disassemble for cleaning. There is a jacket through the outlets of which coolant is supplied to heat or cool the contents of the vessel. A vacuum pump is connected through the refrigerator's vacuum port or vacuum valve to create a vacuum. You can attach a funnel, refrigerator, stirrer, sensors, etc. to the lid. The electronic unit controls the entire operation of the device. Characteristics Valve(s) material PTFE (Teflon). The seals are made from it. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum ≥-0.098 Nutrition 220 V/ 50 Hz Volume, l 2 Mixer power, W 60 Material glass Boro 3.3., photoroplast, steel SS304