INSTALLATION FOR DETERMINING THE RESISTANCE OF MICROSPHERICAL CATALYSTS TO ABRASION ASTM D5757-11

The glass reactor RGPF II from Primelab is a laboratory device of a non-standard shape. The design contains several sections necessary to create the required conditions in laboratory processes. There are two side outlets, at the ends of which olives are provided for a reliable and durable connection to the equipment using soft hoses. The glass reactor RGPF II is a development of the Primelab company, which produces laboratory glassware and instruments to order according to the customer’s technical specifications. The conditions and terms of production depend on the volume of work.

Characteristics Maximum heating temperature, °C up to +200 °С Minimum cooling temperature -120 °C Speed range, rpm 60-600 Shaft diameter, mm 12 Nutrition 220 V Heater power, W 4000 (bath heating) Volume, l thirty Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating Engine power, W 90, 3:1 gear motor

Minimum cooling temperature -120 °C Speed range, rpm 60-1000 Nutrition 220 V Heater power, W 1500 (bath heating) Volume, l 5 Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating 7 mm Engine power, W 90 Maximum plate heating temperature, °C up to +200 °С

The reactor has a modular design, making it easy to disassemble for cleaning. There is a jacket through the outlets of which coolant is supplied to heat or cool the contents of the vessel. A vacuum pump is connected through the refrigerator's vacuum port or vacuum valve to create a vacuum. You can attach a funnel, refrigerator, stirrer, sensors, etc. to the lid. The electronic unit controls the entire operation of the device. Characteristics Valve(s) material PTFE (Teflon). The seals are made from it. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum ≥-0.098 Nutrition 220 V/ 50 Hz Volume, l 2 Mixer power, W 60 Material glass Boro 3.3., photoroplast, steel SS304

Characteristics Valve(s) material PTFE discharge valve Speed range, rpm 60-1000 Shaft diameter, mm 12 Volume, l 50 Mixer power, W 120 W, 3:1 gear motor Vacuum, MPa 0.098 Material Stirrer rod: SS304, PTFE coated blades Housing material and other glass elements - Boro glass (3.3). Dimensions in packaging 140x72x66 cm, 100 kg

The 10 liter SF laboratory reactor is a complete medium-sized unit. In terms of functionality, it is not inferior to large production models. It has a modular design and consists of interchangeable parts. Thanks to this, the reactor can be prepared for a specific task. In particular, you can connect a lot of additional equipment to it: various sensors, a thermostat, a vacuum pump, etc. The design of the device is well thought out and easy to use. The reaction vessel is made of borosilicate glass 3.3. It is equipped with a jacket for supplying coolant and a cover with holes for connection with additional equipment. These include a refrigerator, a vacuum valve, a loading funnel, a top-drive stirrer attachment, a temperature sensor, etc. The operation of the stirrer can be controlled using an electronic control unit. The entire structure is mounted on a steel frame with wheels, and the parts are interconnected with Teflon seals. Characteristics Valve(s) material PTFE discharge valve Speed range, rpm 60-1000 Shaft diameter, mm 12 Volume, l 10 Mixer power, W 90 W, 3:1 gear motor Vacuum, MPa 0.098 Material Stirrer rod: SS304, PTFE coated blades Housing material and other glass elements - Boro glass (3.3). Dimensions in packaging 100x58x66 cm, 70 kg

The unit is designed to simulate and study the processes of delayed coking occurring at elevated temperature and pressure in a stainless steel reactor made in the form of a flask with a spherical bottom and a removable lid. The installation allows you to obtain experimental data, select and optimize the parameters of the technological process, test various variants of raw mixtures, determine the material balance of the process, the characteristics of the process products. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. The power supply is a single-phase AC network with a voltage of 230-240V 50-60 Hz. The average service life of the autoclave is 6 years. TECHNICAL CHARACTERISTICS Operating pressure range, MPa 0÷0.6 Reactor operating temperature range, 0C 50÷550 The discreteness of the temperature setting is 0C 1 Relative error of temperature maintenance, 0C ± 0.2 Reactor material steel 12x18N10T Power consumption, kW not more than 3 Overall dimensions (HxWxD) 1600x1100x495 Weight, kg 240 Continuous operation mode

Characteristics Minimum cooling temperature -120 °C Speed range, rpm 60-600 Nutrition 220 V Heater power, W 3000 (bath heating) Volume, l 20 Vacuum, MPa 0.098 Material stirrer head: stainless steel coated with PTFE 12 mm Engine power, W 90, 3:1 gear motor Maximum plate heating temperature, °C up to +200 °С

The reactor has a modular design, so it can be quickly assembled and disassembled. It has a standard package, which includes a 3-liter reaction vessel with a jacket, two valves, a lid with holes for components, a top-drive stirrer with a nozzle, a 60 W asynchronous brushless motor and a dropping funnel. There is a condenser with a vacuum port and an electronic control unit. These parts are assembled onto a mounting rack, which is attached to a massive platform for the stability of the entire reactor. Characteristics Valve(s) material PTFE (Teflon). This is what the seals are made from. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum ≥-0.098 Nutrition 220 V/ 50 Hz Volume, l 3 Mixer power, W 60 Material glass Boro 3.3., photoroplast, steel SS304

Characteristics Maximum heating temperature, °C up to +200 °С Minimum cooling temperature -120 °C Speed range, rpm 60-600 Shaft diameter, mm 14 Nutrition 220 V Heater power, W 9000 (bath heating) Volume, l 150 Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating Engine power, W 90, 3:1 gear motor

The unit is designed for testing fresh catalysts, deactivated in laboratory conditions and equilibrium (used in industry). The volume of the loaded catalyst is from 5 to 12 grams, the loading of raw materials (vacuum gas oil) is 1-3 grams. Conradson coking capacity should not exceed 10%. After cracking, the degree of coking of the catalyst is determined directly at the installation. Liquid and gaseous cracking products are analyzed by three gas chromatographs with automatic dispensers, which makes it possible to determine the degree of conversion and selectivity of the catalyst.

The 20 liter laboratory reactor is designed to handle various processes involving stirring, heating, distillation and other processes. Most often used to prepare a product from several ingredients under controlled temperature and pressure conditions. Has a high efficiency. It is used in the oil and gas industry, pharmaceuticals, paint and varnish production and other areas. This is due to the fact that the device is made of high-quality materials: all glass parts are made of borosilicate glass 3.3, and the stand is made of stainless steel. The reactor is multifunctional due to its configuration: • Motor with the ability to adjust the rotation speed; • Overhead mixer; • Digital control unit; • Jacketed flask and outlet valve for quick unloading of finished products; • Flask lid with six inlets and Teflon seals; • Drip funnel; • Condenser with receiving flask; • Vacuum valve; • Frame for installation of all auxiliary equipment. The 20 liter reactor is quite easy to disassemble and reassemble for modernization, cleaning and other purposes. Characteristics: • Valve material: PTFE injection valve • Speed range, rpm: 60-1000 • Power supply: 220 V, 50 Hz • Mixer power, W: 90, 3:1 gear motor • Reaction flask volume, l: 20 • Vacuum, MPa: 0.098 • Dimensions in packaging: 122x59x66 cm

The laboratory unit is designed to evaluate the activity of heterogeneous catalysts in a reactor with a fixed bed for the hydrotreating process. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS OF THE HYDROTREATING AND HYDROGENATION UNIT Reactor: 1 piece Reactor volume, 240 ml Material 12X18H10T Inner diameter, mm 24 Length, mm 500 Operating temperature range, 0C 20÷600 Operating pressure range, MPa 0÷10 Removable pocket for thermocouples,mm 600 Reactor furnace: 1 piece Type of furnace Type of furnace Casement Number of thermostatic zones, pcs 3 The length of the full heated zone of the furnace, mm 450 The length of each of the four thermostatic zones, mm 150 The length of the isothermal zone of the furnace, mm 300 The power consumed by each isothermal zone, W 800 Power consumed by all three zones of the furnace, W 2400 The discreteness of the temperature setting, 0C 1 Hydrogen flow rate shaper: 1 piece Type of shaper, RGE Bronkhost Range of supported expenses, l/h 0-100 Inlet pressure, 100 bar Nitrogen flow rate shaper: 1 piece The type of the shaper, the leak (Nat2) Hy-Lok Range of supported expenses, l/h 0-10 Inlet pressure, 0-100 bar Raw material consumption shaper: 1 piece Shaper type, liquid pump KAPPA 10 Supported flow range, ml/min 0-10 Output pressure, 0-400 bar Raw material capacity: 1 piece Volume, l 4 Maximum pressure, atm 4 Working pressure, atm 0.2-1 Raw Materials Oil Installation: 1 piece Operating cycle of the installation, h 120 Inlet gas pressure calculated H2, N2, MPa 10 Actuation pressure of mechanical safety valves, 9.9 MPa Supply voltage 220V 50Hz The power consumption of the entire installation is not more than, kW 3 Installation weight without cabinet, kg 120 Overall dimensions, mm 1800x865x550 Overall dimensions of the cabinet, mm 2000x800x880

Characteristics Valve(s) material PTFE (Teflon). The seals are also made from it. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum 0.098 Nutrition 220 V/ 50 Hz Volume, l 1 Mixer power, W 40 Material Stirrer rod: SS304, PTFE coated blades Housing material and other glass elements - GG17 glass (3.3).

Technical specifications: Operating temperature range, °C 50 ... 175 The discreteness of the temperature setting, °C 0.1 Temperature setting accuracy, °C ± 2 Accuracy of temperature maintenance, °C ± 0.5 Time interval setting range from 1 min to 20 h 59 min Time setting discreteness, min 1 Power consumption, V * A, no more than 450 The size of the landing nest (diameter x depth), mm 17 x 72 Number of landing nests, pcs 29 Overall dimensions, mm, not more than 300 x 300 x 120 Weight, kg, not more than 8