CR-1B Reactor by Tetraquant

Catalytic reforming is used to produce high-octane components of automobile gasoline, flavored concentrate for the production of individual aromatic hydrocarbons, as well as technical water. Isomerization of paraffin hydrocarbons is used to increase the octane number of C5 - C6 oil fractions by converting paraffins of normal structure into their isomers having a higher octane number.oroda. Hydrotreating of distillates is used to improve the quality and stability of light distillates, raw materials of catalytic cracking, as a result of the use of reactions of destructive hydrogenation of organosulfur compounds and hydrogenation of unsaturated hydrocarbons. Catalytic cracking is used to obtain additional amounts of light petroleum products, namely high-octane gasoline and diesel fuel, by decomposition of heavy oil fractions in the presence of a catalyst. Alkylation of isobutane with olefins is used to produce gasoline fractions with high stability and detonation resistance using the reaction of interaction of isobutane with olefins in the presence of a catalyst. Polymerization (oligomerization) of olefins is used to produce low molecular weight polymers (oligomers) of propylene and butylene used as motor fuel or raw materials for petrochemical synthesis. Hydrocracking is used to obtain an additional amount of light petroleum products by catalytic decomposition of heavy raw materials in the presence of hydrogen. Thermal cracking and Visbreaking is used to obtain in the mode of thermal cracking – additional amounts of light petroleum products by thermal decomposition of residues from oil distillation, in the mode of visbreaking – improving the quality of boiler fuel Coking is used to produce petroleum coke and an additional amount of light petroleum products from heavy residues. The raw materials are tar, thermal cracking residue, heavy gas oil. The products are, for example, petroleum coke.

The unit is designed to determine the so-called Davison index (the ratio of catalyst fractions with a particle size of less than 20 microns before and after analysis), which characterizes the abrasion resistance of microspherical catalysts of the cracking process in a fluidized bed. The installation is included in the register of testing facilities.

The unit is designed for testing isobutane dehydrogenation catalysts in the fluidized bed by activity and selectivity, as well as conducting life tests in automatic continuous mode without limiting the number of test cycles. technical specifications Reactor made of titanium or nickel-free steel 800mm long with an internal diameter of 30 ± 1mm with a removable coaxial pocket for three control thermocouples; The furnace is a hinged, four-zone furnace with an operating temperature range from 50 to 800 ° C with a length of 900 mm with an automatic accelerated cooling system necessary for drying the catalyst before testing at a temperature of 300-400 ° C.; A generator of four gas flows (isobutane, nitrogen, air, hydrogen), based on electronic regulators of the mass flow of gas with an error of no more than 0.5%; A gas flow switch that implements the necessary sequence of supply and mixing of gases entering the reactor, pressure monitoring in the reactor necessary to assess the degree of filter clogging, reverse purging of filters to clean them, automatic loading and unloading of the catalyst in nitrogen without the presence of air, as well as automatic filling of the heated reactor with nitrogen during an emergency power outage and hydrogen supply for regeneration; Power supply 230V 50Hz; Overall dimensions 800x800x2000; The installation is placed in a ventilated cabinet with a glass lockable door; Gas flow heater with operating temperature range from 20 to 500C installed if necessary before entering the reactor; Determination of qualitative and quantitative characteristics of the gas mixture at the reactor outlet using a gas chromatograph with an automatic analysis results processing system, with an assessment of activity and selectivity.

The laboratory unit is designed to evaluate the activity of heterogeneous catalysts in a reactor with a fixed bed for the hydrotreating process. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS OF THE HYDROTREATING AND HYDROGENATION UNIT Reactor: 1 piece Reactor volume, 240 ml Material 12X18H10T Inner diameter, mm 24 Length, mm 500 Operating temperature range, 0C 20÷600 Operating pressure range, MPa 0÷10 Removable pocket for thermocouples,mm 600 Reactor furnace: 1 piece Type of furnace Type of furnace Casement Number of thermostatic zones, pcs 3 The length of the full heated zone of the furnace, mm 450 The length of each of the four thermostatic zones, mm 150 The length of the isothermal zone of the furnace, mm 300 The power consumed by each isothermal zone, W 800 Power consumed by all three zones of the furnace, W 2400 The discreteness of the temperature setting, 0C 1 Hydrogen flow rate shaper: 1 piece Type of shaper, RGE Bronkhost Range of supported expenses, l/h 0-100 Inlet pressure, 100 bar Nitrogen flow rate shaper: 1 piece The type of the shaper, the leak (Nat2) Hy-Lok Range of supported expenses, l/h 0-10 Inlet pressure, 0-100 bar Raw material consumption shaper: 1 piece Shaper type, liquid pump KAPPA 10 Supported flow range, ml/min 0-10 Output pressure, 0-400 bar Raw material capacity: 1 piece Volume, l 4 Maximum pressure, atm 4 Working pressure, atm 0.2-1 Raw Materials Oil Installation: 1 piece Operating cycle of the installation, h 120 Inlet gas pressure calculated H2, N2, MPa 10 Actuation pressure of mechanical safety valves, 9.9 MPa Supply voltage 220V 50Hz The power consumption of the entire installation is not more than, kW 3 Installation weight without cabinet, kg 120 Overall dimensions, mm 1800x865x550 Overall dimensions of the cabinet, mm 2000x800x880

The unit is designed to simulate and study the processes of delayed coking occurring at elevated temperature and pressure in a stainless steel reactor made in the form of a flask with a spherical bottom and a removable lid. The installation allows you to obtain experimental data, select and optimize the parameters of the technological process, test various variants of raw mixtures, determine the material balance of the process, the characteristics of the process products. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. The power supply is a single-phase AC network with a voltage of 230-240V 50-60 Hz. The average service life of the autoclave is 6 years. TECHNICAL CHARACTERISTICS Operating pressure range, MPa 0÷0.6 Reactor operating temperature range, 0C 50÷550 The discreteness of the temperature setting is 0C 1 Relative error of temperature maintenance, 0C ± 0.2 Reactor material steel 12x18N10T Power consumption, kW not more than 3 Overall dimensions (HxWxD) 1600x1100x495 Weight, kg 240 Continuous operation mode

Laboratory installation for modeling the process of thermal contact cracking (TCC) of heavy oil residues (TNO) (heavy oil fuel oil, tar and semi-tar, asphalt of the process of de-asphalting of high-viscosity oils, cracking residue or pitch, heavy gas oil, natural bitumen, etc.) with a movable solid coolant. technical specifications Operating pressure range, MPa 0÷4 Reactor operating temperature range, 0C 50÷800 Reactor inner diameter, mm, 31 Reactor length, mm, 875 Number of thermostatically controlled independent zones 4 Length of each independent isothermal zone of the furnace, mm 200 The length of the full isothermal zone of the furnace, mm 800 Thermocouple Pocket Availability The type of furnace is Casement The power consumed by each independent thermostatically controlled zone of the furnace, W 720 Power consumed by all four zones of the furnace, W 2880 The discreteness of the temperature setting, 0C 1 The flow range of the liquid pump, ml/min 0.1-10 The maximum pressure of the high-pressure liquid pump, not less than 20 MPa Flow range N2, l/min 0÷20 Pressure in the low pressure lines N2 and air, MPa ≤0.6 Operating temperature range of the evaporator-mixer of raw materials, sup>0C 50÷500 Actuation pressure of mechanical safety valves, MPa 3 Maximum pressure in the raw material container, 0.1 MPa Supply voltage 230-240V 60Hz The power consumption of the installation is not more than 3.5 kW The discreteness of the temperatures and flow rates displayed on the displays is 0.1 Installation weight without cabinet, kg 100 Overall dimensions of the installation, mm 1900x865x550 Overall dimensions of the cabinet, mm 2000x880x800 The technical characteristics of the purchased units used in the installation are given in the technical documentation for these units supplied with the installation The length of the supply pipelines, m 10 The coolant of the refrigerator "tosol"

An automated installation for determining the wear of various catalysts, including KPS (FCC) for cracking with a fluidized bed by an air jet and is designed to determine the comparative wear characteristics of the KPS (FCC) of the catalyst by friction of an air jet according to ASTM D5757-11. It is used for testing with irregularly shaped spherical sludge particles (size from 10 to 180 microns). Abrasion is achieved by fluidization of the sample under the influence of jets of moist air. The percentage of fine particles (less than 20 microns in size) after a 5-hour test is an air jet abrasion index (AJI). technical specifications The range of operating air pressures for the power supply of the installation is 0.8±0.1 MPa The range of air flow rates for the power supply of the installation is not less than (l/min) 20 Absolute error of the air flow rate maintained automatically at a flow rate of 10 l/min. no more, l/min. ± 0.05 Power consumption not more than 0.2 kW Overall dimensions, mm and weight kg. 560x760x1700, 30 Abrasion pipe made of steel 12x18 n10t with dimensions, mm 710±10, 35 ± 0.5 Three sapphire nozzles with a diameter and length, mm 0.381±0.005, 2±1.0 Continuous operation mode Control: microprocessor with tactile control for setting the display and automatic maintenance of installation parameters and mathematical processing of analysis results 60 The convergence of the results when testing the same catalyst is not more than 0.1%

The unit is designed for testing fresh catalysts, deactivated in laboratory conditions and equilibrium (used in industry). The volume of the loaded catalyst is from 5 to 12 grams, the loading of raw materials (vacuum gas oil) is 1-3 grams. Conradson coking capacity should not exceed 10%. After cracking, the degree of coking of the catalyst is determined directly at the installation. Liquid and gaseous cracking products are analyzed by three gas chromatographs with automatic dispensers, which makes it possible to determine the degree of conversion and selectivity of the catalyst.

The bench laboratory unit is designed to test the adsorption properties of silica gels, protective layers and selective hydrogenation catalysts. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Power supply – three- or single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz.; air 0.4 — 0.8 Mpa. The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS Operating pressure range, MPa 0÷6 Reactor operating temperature range, 0C 20÷600 Reactor inner diameter, mm 20 Internal length of the reactor, mm 690 A thermocouple pocket with a movable filter and a support grid fixed on it to regulate the volume of the tested catalyst. Length of the isothermal zone, mm 300 The type of furnace is Casement Number of thermostatically controlled independent zones 4 The power consumed by each of the four independent thermostatic zones, W ≤ 400 The discreteness of the temperature setting, 0C 0.1 Flow range C2 H4, l/min 0,02÷1,7 Flow range C3 H6, l/min 0,02÷1,7 Flow range H2, l/min 0÷0.02 Flow range N2, ml/min 0.02÷1.7 Actuation pressure of mechanical safety valves, 6,8 MPa Supply voltage 220V 50Hz Power consumption not more than, kW 5 The discreteness of the temperatures and flow rates displayed on the displays is 0.01 Installation weight, kg 230 Overall dimensions of the installation, mm 1680x1480x580 Length of supply gas pipelines, m 20

Technical specifications: Operating temperature range, °C 50 ... 175 The discreteness of the temperature setting, °C 0.1 Temperature setting accuracy, °C ± 2 Accuracy of temperature maintenance, °C ± 0.5 Time interval setting range from 1 min to 20 h 59 min Time setting discreteness, min 1 Power consumption, V * A, no more than 450 The size of the landing nest (diameter x depth), mm 17 x 72 Number of landing nests, pcs 29 Overall dimensions, mm, not more than 300 x 300 x 120 Weight, kg, not more than 8

Monophase gas (the phase state of reagents at room temperature is liquid or gas). Monophase liquid (the phase state of reagents at room temperature is liquid). Two-phase (gas-liquid heterophase system). Temperature: operating range 500C – 6000C, 8000C.(three-zone heating furnace). Pressure: operating range 0.1 – 60, 100, 200 MPA. In the photo: A universal bench laboratory installation for the study of basic organic synthesis processes in a reactor with a fixed catalyst layer The unit is designed (tested) for the study of a wide range of heterogeneous catalytic reactions, including: Hydrogenation processes in the gas phase. Hydrogenation processes in the liquid phase. Gas-phase dehydration of aliphatic and aromatic alcohols. Dehydration of aromatic alcohols in the liquid phase. Alkylation of aromatic hydrocarbons with olefins and alcohols. Hydroalkylation of aromatic compounds with ketones. Dehydrogenation of chemical compounds of various classes.

The glass reactor RGPF II from Primelab is a laboratory device of a non-standard shape. The design contains several sections necessary to create the required conditions in laboratory processes. There are two side outlets, at the ends of which olives are provided for a reliable and durable connection to the equipment using soft hoses. The glass reactor RGPF II is a development of the Primelab company, which produces laboratory glassware and instruments to order according to the customer’s technical specifications. The conditions and terms of production depend on the volume of work.