UNIVERSAL BENCH LABORATORY INSTALLATION FOR THE STUDY OF BASIC ORGANIC SYNTHESIS PROCESSES IN A REACTOR WITH A FIXED CATALYST LAYER

• Consists of a mirror telescope coupled with a Fourier spectrometer and a searchlight with an IR emitter • Used to register the spectra of gas and aerosol-gas mixtures on routes up to 100 meters long • The diameter of the main mirror of the telescope is 170 mm • Angular field of view +/- 3 degrees. • An additional reflector can be included in the kit

The gas chromatograph "Kristallux-4000M" is fully automated, starting from sample input and ending with chromatographic information processing, including the functions of automatic temperature control of thermostats, flow rates and pressure of the carrier gas (EUPG system), auxiliary gases, automatic ignition of detectors, flame burning control during operation, measurement of detector signals using Gorenje 24-bit ADC. Technical specifications: The detection limit of PID is 1,1x10-12 gS/s for h-hydrocarbons 1,1x10-12 gS/s for propane. The detection limit of DTP1.7x10-14 g/s for lindane 3.9x10`15 g/s for lindane (micro-ED) The detection limit of EZD1x10`13 grus for phosphorus in metaphos 8x10`13 g5/s for sulfur in metaphos or hydrogen sulfide PFD detection limit 1.5x10`14 g/s for phosphorus in metaphos 3x10`13 GM/s for nitrogen in azobenzene Detection limit of TID2x10`10 g/ml by hydrogen The detection limit of TcD is 5x10`13 g/s for benzene The detection limit of the FEED is 3x10`13 g/s for carbon in methane 3x10`13 g/s for carbon in methane Detection limit GID500:1 (M7-801) with the introduction of 1x10`12 g / ml of octafluoroaphthalene The signal-to-noise ratio of MSD 1500:1 (Maestro-oMS) when entering 1x10`12 g / ml of octafluoroaphthalene Linear dynamic range of PID x1*107 Linear dynamic range DTP1*108 The volume of the column thermostat is 14 (19)l The temperature of the column Current.Wednesday +3 °C to +400 °C (by special order up to 450 °C) (by special order from -10°C with use. cold. ust-ki)(by special order from -100 °C. with use. liquid, no.) The discreteness of the temperature setting is 0, ° C Temperature stability 0.01 °C Temperature programming speed 0t 0.1 to 125 °C/min (by special order up to 150 °C/min) The number of isotherms is not less than 30 The cooling rate of the column thermostat is from 400 to 50 °C3.3 min. The maximum temperature of the detector and evaporator is 450 °C Carrier gas consumption from 0 to 100 ml/min.(by special order up to 500 ml/min.) Carrier gas pressure (for capillary column) from 0 to 0.40 Mpa (by special order up to 1 MPa) The maximum inlet gas pressure on a special order is 0.5 MPA 1.25 MPA Hydrogen consumption 0-500 Air consumption 0-1000 Overall dimensions (width x depth x height) 550%500*500 mm Weight 39 kg Electric power supply from AC mains voltage (220.2) V, frequency (50 +1) Hz The maximum power consumption (in steady-state mode) is 900 VA.

Technical specifications: Sensitivity (minimum thickness of recorded oil films) from 0.5 microns The root-mean-square slope of the water surface up to 20 ° Distance from the receiving device up to 1000 m Sensor power supply 100-240 V, 50-60 Hz Power consumption up to 3 watts Ambient air temperature from -10 to +50 °C Humidity up to 100% (rain) Distance to the water surface 0.5–20 m Dimensions 120x180x120 mm Weight up to 1.5 kg

The UKK-6 cryoconcentration unit (hereinafter referred to as UKK-6) is an integral part of an automated chromatographic complex based on the Kristallux-4000M gas chromatograph and is designed to control the quality of 6.0 grade helium and 6.0 grade hydrogen for the presence of micro-impurities of Ne, CH4, O2+Ar, N2, CO, CO2 and H2.AUKK-6 concentrates gaseous impurities (Ne, H2, O2+Ar, CH4, CO and CO2) in helium and hydrogen in sorption columns at liquid nitrogen temperature, followed by focusing and thermal desorption of accumulated impurities and introducing them into a gas chromatograph to determine their qualitative and quantitative composition. technical specifications The analyzed gas is Helium, hydrogen Temperature of sorption columns during adsorption, 0C -196 Maximum temperature of thermal desorption, 0C 400 The pressure of the analyzed gas, not more than 0.4 MPa Inlet gas pressure, not more than 1.0 MPa Total analysis time, no more than 17 minutes Volume of a vessel with liquid nitrogen, l 6 Automatic replenishment (topping up) of liquid nitrogen before each concentration cycle - Supply voltage 230-240V, 50-60Hz Power consumption, no more than W0C 2000 Overall dimensions (WxDxH), mm 30 Weight, not more than 0.02-1.7 kg

The spectrometer was created according to the Cherni-Turner scheme based on a flat diffraction grating and an MAES analyzer with one line of photodetectors. It has increased photometric accuracy due to cooling and temperature stabilization of the photodetector range, as well as due to its shell-less design, in which there is no re-reflection of radiation on the cover glass and the background level in the recorded spectrum decreases. The optical scheme and design of the spectrometer are optimized to obtain a high-quality spectrum with a low level of background radiation in any of the regions lying in the spectral range of 190-1100 nm. The choice of the working area is carried out by changing and rotating the diffraction gratings. The sealed case of the spectrometer is filled with an inert gas. The radiation is injected into the spectrometer using a quartz capacitor or a fiber-optic cable with an SMA-905 connector. The optical scheme and design of the spectrometer are protected by patents.

The ultimate display quality is ensured by the use of built-in acoustic and vibration isolation, thermal stabilization, the industry's best sensitivity of the optical recording system and the unique design of the scanning probe system, which allows achieving atomic resolution in routine measurements. In the basic configuration, 50+ AFM techniques are available, including the HybriD method, which allows conducting all cutting-edge nanomechanical, electrical and magnetic studies. Intelligent ScanTronic™ algorithm for one-click optimization of scanning parameters, which allows for perfect relief measurements using the amplitude-modulation method, regardless of the operator's experience. Automated examination of multiple samples using a simple user interface to create a point-by-point scanning scenario and a database for stored received images. Control of samples with dimensions up to 200×200 mm and thickness up to 40 mm at any point of the surface with a positioning accuracy of 1 micron. Wide customization possibilities: installation of additional optical equipment, development of specialized sample holders, combination with a transport system, automation of measurements and data analysis in accordance with customer requirements.

Technical specifications: The range of detectable concentrations 0.025-1.0 and 0.1- 10 mg/l from 10 to 100 mg/l –can be used as an alarm The temperature of the analyzed flow is from + 4 to + 50 °C The pressure in the flow is 0.1-10 atm. Number of measurements per hour 1-4 Output of results Digital scoreboard, RS485, RS232, 4-20 mA current loop Display modes NORM, ALARM, LIMIT Version B1, P1, N1 according to GOST 12997-84 Category of climatic performance UHL4 according to GOST 15150-69 Ambient temperature from + 5 to + 50 °C Relative humidity at + 25 °C 80% Atmospheric pressure 84-106.7 kPa The amplitude of external vibrations with a frequency of 10-55 Hz is not more than 0.15 mm Power supply 187-242 V, 50 ± 1 Hz from an autonomous source, 12 V Power consumption not more than 100 watts Dimensions 600x600x250 mm Weight 50 kg The warranty period of operation is 1 year Average service life of at least 5 years Average time to failure of at least 20,000 hours

Characteristics Valve(s) material Standard: chloroprene copolymer NO-68-1 (TU 38 0051166-98) A country Russia Overall dimensions, L×W×H, mm 322x140x200 Protection class acc. to DIN EN60529 IP20 Noise level, dB 75 dBA Nutrition 230 V, 50 Hz Material working chamber PTFE (fluoroplastic) Ultimate vacuum, mbar abs. 10 for serial, 50 for parallel, 50x2 for independent connection Excess pressure, bar. Maximum permissible excess operating pressure 0.5 bar Productivity, l/min 76 with parallel, 38 with serial, 38x2 with independent connection Maximum current, A 1.2 Equipment Vacuum pump, cable, instructions, passport, packaging (vacuum regulator and spare parts are not included in the kit and must be ordered separately). Device weight, kg 8.6

Nitrogen generators are designed to create an inert atmosphere, fill low-pressure tanks, "rinse" test tubes with inert gas and other applications that require a large, by laboratory standards, nitrogen consumption with reduced requirements for its purity. Technical specifications Volume fraction of nitrogen is not less than % by volume (including impurities of inert gases — argon, neon, helium) 99.6 Volume fraction of oxygen is not more than, % vol. 0,4 Volume fraction of water vapor is not more than, % vol. 0.002 (20 ppm) Maximum nitrogen capacity is at least 200 (3.33 l/min), l/h Maximum nitrogen outlet pressure is not less than 3.5 ati The time of setting the operating mode for single-shift operation is no more than 30 min Nominal inlet air pressure is 6 ati Maximum allowable inlet air pressure is 8 ati Minimum inlet air pressure is 5 ati Compressed air consumption, at nominal inlet pressure and maximum flow rate is no more than, l/h, 1200 (20 l/min) Power consumption is not more than, VA, 100 Overall dimensions (width x depth x height) are not more than, mm, 230x525x510; Weight is not more than 26 kg Working conditions: ambient temperature, C°, from +10 to +35 Electric power supply from single-phase AC mains voltage, V, 220± 10% and frequency, Hz, 50 ± 1 Average full service life is at least 6 years The generator for electrical safety meets the requirements of Class 1, type H according to GOST 12.2.025-76

Technical specifications: Operating spectral range, nm from 190 to 360 Limits of permissible absolute error of wavelength setting, nm ± 5 Detection limit of anthracene (wavelength 252 nm), ng/cm3, no more than 1 The limit of the permissible value of the relative mean square deviation of the output signal (n =5), % of the retention time over the peak area of 1.5 2 Limits of the permissible value of the relative change in the output signal (peak area) for 4 hours of continuous operation, % ± 5 Overall dimensions (LxWxH), mm, no more: 270x420x190 Weight, kg, not more than 9.5 Power consumption, V· A, not more than 50

Technical specifications: LM-3 operating range 220-650 nm LM-4 operating range 220-900 nm Diffraction grating (replica) 1200 strokes per millimeter Radius of curvature DR 125 mm The area of maximum energy concentration is 300-400 nm Inverse linear dispersion in the specified spectral range of 6.7 nm/mm Relative opening 1:3.3 The slits are fiber optical fibers with a diameter of 200 microns, stacked in 1 row. The height of the slots is 5 mm The resolution of the monochromator with the specified slits in the ranges of 220-650 nm is not worse than 1.5 nm The resolution of the monochromator with the specified slits in the range of 650-900 nm is not worse than 2.5 nm The accuracy of the wavelength setting is not worse than 0.2 nm Dimensions no more than 205x125x150 mm Weight not more than 3 kg Supply voltage 90-120 / 187-242 V Power consumption not more than 12 W Current frequency 50/60 Hz

Designation SNOL 11.47.4/2.5 P I2 Temperature, oS 250 Camera power, kW 16 Mandrel length 1200...4600 Opening the lid electric drive

The multifunctional X-ray diffractometer DRON-8 (8H) with a vertical theta goniometer and the horizontal position of the sample allows X-ray diffraction analysis of the phase composition, structural state and orientation of a wide range of objects of various shapes and sizes.

Implements a thermogravimetric (air-thermal) method for determining the mass fraction of moisture, based on measuring the mass of the sample of the analyzed substance before and after drying, followed by calculating the values of the mass fraction of moisture. Air-thermal measuring installations ASESH-8 are registered in the State Register of Measuring Instruments under No. 58526-14, have a certificate of approval of the type of measuring instruments OC.C.31.005 And No. 56847.The installations undergo initial verification and have the appropriate certificate. General characteristics: - The presence of two independent drying chambers. - Possibility of simultaneous determination of humidity of 12 samples: Each drying chamber of the installation consists of 6 independent cells. You can put 2 buckets in each cell. Total capacity of the ASES Installation-8-2 – 24 bucs. - Convenient access to the cells of the drying chamber: On the front side of the cabinet there are four doors for access to the cells. - Natural ventilation: The absence of rotating elements ensures absolute noiselessness of operation and a long service life. - Built-in timer: The ASESH-8-2 installation has 4 timers, by means of which the end of the drying process is monitored in each section with the output of an audible signal and a light indication. - The output to the operating mode is 30 minutes: The power of air-thermal installations is 1200 watts. When entering the operating mode, the power consumption is the same as that of similar cabinets with low power. SCOPE OF DELIVERY : 1. Installation of ASESH-8-2 2. AO-3 cooler 3. Auxiliary accessories 4. Air-heat control unit: 5. Interface unit for connecting a personal computer with a scale (available on request); 6. software for processing and archiving measurements of humidity determination data; The program allows you to: Set the operating temperature in the chambers via a personal computer Set the necessary parameters of the sample drying process according to the selected method Display all current processes (predrying, drying, cooling) and parameters (temperature, time) during the tests. To monitor the process by means of an electronic timer with the output of an audible signal. Record all weighing results. Perform humidity calculations in accordance with standardized methods. To calculate the humidity with pre-drying, the program uses formulas that allow you to get an accurate result. Archive and print test results. According to the test results of FSUE "UNIIM", it is recommended to use a laboratory mill of the BLIZZARD series for sample preparation. SCOPE OF APPLICATION: 1. Crop production, agriculture and forestry. 2. Products of meat, dairy, fish, flour-milling, feed and microbiological industries. 3. Food industry products. 4. Cellulose, paper, cardboard and products made from them. 5. Medicines, chemical and pharmaceutical products and medical products. 6. Building materials. 7. Products of the logging and sawmilling and woodworking industry. 8. Ground, soils, mineral fertilizers. Technical specifications: The measurement range of the mass fraction of moisture, % from 0.5 to 80 Operating temperature range, °C from 45 to 160 The error of setting and maintaining the temperature in the working area, ° C, not more than 2.0 Limits of permissible absolute error, % ± 0.5 Power consumption, V• A, not more than 1200 Overall dimensions, mm 240 × 260 × 640 Overall dimensions of the cell, mm 75 x 40 x 165 (depth) Weight, kg 28.4

The GA-400-N nitrogen generator (hereinafter referred to as the generator) is a modification of the GA-400 nitrogen generator and is designed primarily to work with a storage tank (receiver) in which a certain "reserve" of nitrogen can be created. Unlike the GA-400, the GA-400-H generator has a built-in pressure monitoring system for nitrogen accumulated in the receiver, which puts the generator into "standby" mode when the maximum pressure value is reached in the receiver, and restarts the generator when the pressure drops below the minimum value. This work allows you to reduce energy consumption and increase the service life of the compressor feeding the generator. Technical specifications Volume fraction of nitrogen is not less than 99.5% by volume (including impurities of inert gases — argon, neon, helium) Volume fraction of oxygen is not more than 0.5 % vol. Volume fraction of water vapor is not more than 0.002 % vol.(20 ppm) Maximum nitrogen capacity, with nitrogen pressure in the storage tank below 2 ati, is not less than 400 l/hour (6.66 l/min) Nominal inlet air pressure is 6 ati Maximum allowable inlet air pressure is 8 ati Minimum inlet air pressure is 5.5 ati Compressed air consumption, at nominal inlet pressure and maximum flow rate is no more than 3000 l/h (50 l/min) Factory setting of the maximum pressure value in the storage tank is 3.5± 0.2 ati Factory setting of the minimum pressure value in the storage tank is 2.4 ±0.4 ati Power consumption is not more than 100 VA Overall dimensions, (width x depth x height) are not more than 230x580x680 mm; Weight is not more than 35 kg Working conditions: ambient temperature, C°, from +10 to +35 Electric power supply from single-phase AC mains voltage, V, 220± 10% and frequency, Hz, 50 ± 1 Average full service life is at least 6 years The generator for electrical safety meets the requirements of Class 1, type H according to GOST 12.2.025-76

The AP-35 analyzer is a fully automated analytical complex designed for continuous X-ray fluorescence analysis of the chemical composition of slurries and solutions in flow. The instrument has a movable software-controlled measuring head with an X-ray tube and fixed spectrometric channels (up to 8), each of which can be set up for any chemical element (from Ca to U). In operation, up to 15 flow cells are measured by the head according to a preset program. Multi channel capability (up to 15 products to be measured). Compatibility with automation systems for sampling, sample delivery, data handling and presentation, data archiving. Link to factory process control system High expressiveness, high analytical precision, low detection limits, reproducibility High reliability. The principle of operation is based on the excited fluorescence produced by the atoms of the material under analysis through the radiation of an X-ray tube. The fluorescence radiation of a particular chemical element is picked up by the crystal analyzer, and then the radiation at a specific wavelength is detected by an X-ray tube detector. The intensity of the recorded fluorescence radiation of a certain wavelength is directly proportional to the mass fraction of the chemical element in the substance under study.

The PL.HM03.01.60 Primelab vacuum diaphragm pump is suitable for creating a vacuum up to 60 mbar and a flow rate of 38 l/min. It has a dry design that does not require lubrication. Quite easy to use and does not create any inconvenience during operation. Its noise level does not exceed 75 dB. With a light weight of 6.9 kg, it has compact dimensions (289.5x160x200 mm), allowing the pump to be integrated into an already equipped space. Complies with IP20 protection class. The PL.HM03.01.60 Primelab vacuum diaphragm pump is supplied in the following package: vacuum pump, cable, instructions, passport, packaging (vacuum regulator and spare parts are not included in the kit and must be ordered separately). Warranty and post-warranty service is available in Russia.