UNIVERSAL BENCH LABORATORY INSTALLATION FOR THE STUDY OF BASIC ORGANIC SYNTHESIS PROCESSES IN A REACTOR WITH A FIXED CATALYST LAYER

The Primelab vacuum diaphragm pump PL.HM01.01.8 has excellent performance - up to 38 l/min at a maximum vacuum of 8 mbar. Suitable for a wide range of industrial and laboratory applications. It is used for working with chemically active substances due to the use of high-quality materials in its design that do not react with toxic reagents. The chambers are made of fluoroplastic, all parts have a fluoroplastic coating. Complies with IP20 protection class. Supplied complete with equipment sufficient for quick assembly and operation of the device. Namely this: vacuum pump, cable, instructions, passport, packaging (vacuum regulator and spare parts are not included in the kit and must be ordered separately).

Technical specifications: LM-3 operating range 220-650 nm LM-4 operating range 220-900 nm Diffraction grating (replica) 1200 strokes per millimeter Radius of curvature DR 125 mm The area of maximum energy concentration is 300-400 nm Inverse linear dispersion in the specified spectral range of 6.7 nm/mm Relative opening 1:3.3 The slits are fiber optical fibers with a diameter of 200 microns, stacked in 1 row. The height of the slots is 5 mm The resolution of the monochromator with the specified slits in the ranges of 220-650 nm is not worse than 1.5 nm The resolution of the monochromator with the specified slits in the range of 650-900 nm is not worse than 2.5 nm The accuracy of the wavelength setting is not worse than 0.2 nm Dimensions no more than 205x125x150 mm Weight not more than 3 kg Supply voltage 90-120 / 187-242 V Power consumption not more than 12 W Current frequency 50/60 Hz

Meta-Chrome Research and Production Company LLC presents a multifunctional device "PTI-1", which allows to determine the resistance of granular catalysts and adsorbents to friction and abrasion according to SPENCE and ASTM D4058 standards. The error of maintaining the speed, rpm: ± 0.3 Digital Control (controller) Power Supply: 100-240 V, 50/60Hz Power consumption: 18W Permissible sample weight: No more than 100 g. Device weight: 12.5 kg with cylindrical nozzle 10.8 kg with drum nozzle Overall dimensions with cylindrical nozzle, cm: 38,9x31,4x45,9 Overall dimensions with a drum nozzle, cm: 48,5x30,4x45,4 Dimensions of the sieve cells according to the ASTM method, mm: ASTM No20 0.85 The dimensions of the sieve cells according to the SPENCE method, mm: 2/3 of the minimum size of the granules. At the request of the customer. Scales on request of the customer Operating conditions of UHL 4.2 Ambient temperature from 10 ° C to 35 ° C Relative humidity of the air at a temperature of 25C, % no more than 80% Atmospheric pressure from 84 to 107 kPa (from 630 to 800 mmHg)

Technical specifications: The minimum limit of operation is 3×10-4 mg/m3 (the average daily MPC of a residential premises in accordance with GN 2.1.6.1338-03 of May 21, 2003) The range of set thresholds is from 3×10-4 mg/m3 to 1×10-3 mg/m3 Measurement time, no more than 15 s Output signals ON, READY, DANGEROUS, FAULTY Electrical parameters of the output signal 0-24 V, 0.5 A Operating mode Monitoring Average full service life of 5 years Frequency of maintenance 1 time in 3 months RS-232 digital output Power supply 190-240 V, 50 Hz Power consumption, no more than 30 watts Overall dimensions, no more than 280x420x600 mm Weight, not more than 18 kg

The UKK-6 cryoconcentration unit (hereinafter referred to as UKK-6) is an integral part of an automated chromatographic complex based on the Kristallux-4000M gas chromatograph and is designed to control the quality of 6.0 grade helium and 6.0 grade hydrogen for the presence of micro-impurities of Ne, CH4, O2+Ar, N2, CO, CO2 and H2.AUKK-6 concentrates gaseous impurities (Ne, H2, O2+Ar, CH4, CO and CO2) in helium and hydrogen in sorption columns at liquid nitrogen temperature, followed by focusing and thermal desorption of accumulated impurities and introducing them into a gas chromatograph to determine their qualitative and quantitative composition. technical specifications The analyzed gas is Helium, hydrogen Temperature of sorption columns during adsorption, 0C -196 Maximum temperature of thermal desorption, 0C 400 The pressure of the analyzed gas, not more than 0.4 MPa Inlet gas pressure, not more than 1.0 MPa Total analysis time, no more than 17 minutes Volume of a vessel with liquid nitrogen, l 6 Automatic replenishment (topping up) of liquid nitrogen before each concentration cycle - Supply voltage 230-240V, 50-60Hz Power consumption, no more than W0C 2000 Overall dimensions (WxDxH), mm 30 Weight, not more than 0.02-1.7 kg

The spectrometer is designed to determine the contents of elements in the range from Na to U in substances in solid, powdery, dissolved states, as well as deposited on the surface or deposited on filters. The principle of operation of the X-ray spectrometer is based on irradiation of the sample with primary radiation from an X-ray tube, measurement of the intensity of secondary fluorescent radiation from the sample at wavelengths corresponding to the elements to be determined, and subsequent calculation of the mass fraction of these elements according to a pre-constructed calibration characteristic, which is the dependence of the content of the element to be determined on the measured intensity. Secondary fluorescent radiation is decomposed into a spectrum using a crystal analyzer. Due to this, the X-ray fluorescence spectrometer has a high resolution, and therefore the ability to accurately analyze complex multicomponent substances.

Technical specifications: The range of detectable concentrations is 0.04-2 mg/l The temperature of the analyzed flow is from + 5 to + 50 °C The pressure in the flow is 0.1-10 atm. Number of measurements per hour 1-4 Output of results Digital scoreboard, RS485, RS232, 4-20 mA current loop Display modes NORM, ALARM, LIMIT Version B4, P1, N1 according to GOST 12997-84 Category of climatic performance UHL4 according to GOST 15150-69 Ambient temperature from + 5 to + 50 °C Relative humidity at + 25 °C 80% Atmospheric pressure 84-106.7 kPa The amplitude of external vibrations with a frequency of 10-55 Hz is not more than 0.15 mm Power supply 187-242 V, 50 ± 1 Hz from an autonomous source, 12 V Power consumption 100 W Dimensions 600x600x250 mm Weight Not more than 50 kg The warranty period of operation is 1 year Average service life of at least 5 years Average time to failure of at least 10,000 hours

Adsorption nitrogen plant is a set of equipment for the production of nitrogen from atmospheric air by short–cycle heat-free adsorption at a pressure of up to 13 bar. The adsorption nitrogen plants of the Provita company allow to produce nitrogen with a purity of up to 99.9999%. The capacity of the plants ranges from several liters per minute to hundreds of cubic meters per hour. The basis of the installations are nitrogen adsorption generators developed and manufactured by our company. A carbon molecular sieve with a developed microporous structure is used as an adsorbent. The gas generator requires dry compressed air with a pressure of at least 6 bar to operate, so the installation includes an air compressor, as well as a dehumidifier and an air receiver (if they are not part of the compressor). The source air must be cleaned of dust and oil, which is carried out by the main filters included in the installation or directly by the nitrogen generator. The nitrogen receiver is used for the accumulation of production gas.

High-pressure syringe pump (NSHVD-1) with a continuous highly stable fluid flow in a wide flow range of 0.01-10ml/min. with the functions of introducing a correction factor after calibration, setting the volume or pumping time, displaying the amount of pumped, temporary suspension of pumping with automatic resumption, the ability to adjust the flow and volume of the pumped liquid during operation without stops, automatic shut-off of the pump when the set maximum pressure is exceeded, remote control, compensation for changes in the mass flow rate of the liquid pumped by the pump when its temperature changes. TECHNICAL CHARACTERISTICS Flow range, ml/min 0.01 - 10 Dosing error, % 0.2 The discreteness of the task, % 0.01 Maximum working pressure, 12 bar Lifting height of the suction fluid, m2 Accuracy of pressure measurement, % 0.2 The maximum liquid temperature is 60 °C Modbus RTU communication interface Power supply AC 220 V, 50 Hz Dimensions: W x D x H, mm 140 x 335 x 270 Materials in contact with the pumped liquid glass, fluoroplast, stainless steel 316 L

Technical specifications: The time of one measurement is not more than 60 seconds Output of results to digital display board, RS485, RS232; current loop 4-20 mA, (0-20) mA The pressure in the flow is 0.1-10 atm. The range of detectable concentrations of suspended particles is 0.02-5 SCAT-1(VC); 0.1-100 SCAT-1(n) mg/l Execution B4, P1, N1 according to GOST 12997-84 Category of climatic execution UHL4 according to GOST 15150-69 Relative humidity at +25 ° C is not more than 80% The error of photometry per channel is not more than 1% The size of the analyzed microparticles is 0.5-50 microns Display modes NORM, ALARM, LIMIT The temperature of the analyzed flow is from +0.5 to +50 °C Ambient temperature from +0.5 to +50 °C Atmospheric pressure 84-106.7 kPa The warranty period of operation is 1 year Average service life of at least 5 years Dimensions 300x400x150 mm Weight not more than 20 kg Power supply 187-242 V, 50 ± 1 Hz from an autonomous source, 12 V Power consumption 100 W

The generator is designed to produce hydrogen of the highest purity used to power analytical instruments (chromatographs, gas analyzers, etc.). Technical specifications Purity of hydrogen in terms of dry gas is about 99.998% The concentration of water vapor at 20 OC and 1atm is not more than 10 ppm In the output pressure stabilization mode The range of the specified output pressure of hydrogen is from 1.5 to 6.1 ati Stability of the output pressure of hydrogen is not worse than ± 0.02 ati Maximum hydrogen capacity reduced to normal conditions is 36 l/h The time of setting the operating mode, with the output turned off is no more than 20 minutes In the performance stabilization mode: The range of the specified hydrogen performance is from 0 to 36 l/h Maximum developed pressure in performance mode is 5.0 ati Volume of distilled water to be poured is 1.0 l Distilled water consumption is not more than 0.06 l/hour Water consumption is 2.4 g/l of hydrogen The average life of a replaceable deionization filter cartridge (at maximum performance and single-shift operation) is at least 0.5 years Average power consumption: in stationary mode is no more than 250 VA maximum (at startup) is no more than 300 VA Overall dimensions of the generator, (width x depth x height) are not more than 230x470x450 mm The mass of the generator is not more than 18 kg Operating conditions: ambient temperature, °C, from +10 to +35 powered by single-phase AC voltage, V, 220 (+10 -15)% and frequency, Hz, 50 +1 The generator for electrical safety meets the requirements of Class 1, type H according to GOST 12.2.025-76

Main features and benefits: - The compact and ergonomic design of the mixer body allows it to be used not only in stationary laboratories, but also in mobile mobile stations. - The submersible type device is ideal for a wide range of laboratory work. - Intuitive system for smooth power adjustment via the handle. - Start and stop the device using just one button located on the front panel, providing excellent ease of use. - The built-in temperature sensor automatically turns off the mixer if there is a risk of motor overheating, ensuring safety and reliability in operation. Structure and operation of the device: - The device is made in the form of a compact block made of a plastic case, which makes it light and convenient to use. - On the front panel of the device there is a potentiometer knob with a switch and an LED indicator. - On the back of the case there is a hole with a diameter of 7 mm for installing a bracket and a connector for connecting a power supply. - The lower part of the device is equipped with a three-jaw chuck on a hollow shaft. - The top of the device has a hole for the shaft of the mixing nozzle, which allows you to change the height of the nozzle without moving the device up or down if it is installed on a tripod. - The device also has the function of overload protection and complete shaft locking, which ensures its long service life and protects it from unpleasant situations. Primelab is an innovative and user-friendly overhead drive mixer developed in Russia. Thanks to its technological capabilities and ease of operation, it will become an indispensable tool for achieving high quality and efficient mixing of viscous and dense liquids in various fields of industry and scientific research. Characteristics Device overload protection Eat Max. viscosity of the stirred sample, mPa*s 10,000 Maximum torque, Ncm 45 A country Russia Control type analog Mixer shaft diameter max., mm 0.5-10 Motor type Brushless, DC Speed range, rpm 20-2200 Overall dimensions, L×W×H, mm 182x61x200 Protection class acc. to DIN EN60529 IP44 Sample volume (water) 20 liters Display absent Timer absent Engine power, W 53 Power consumption, W 24 Device weight, kg net/gross, kg 2.0/3.2 Supply voltage, V 200–240 Current frequency, Hz 50 Overheat protection (shutdown) Eat The device is supplied with: 1) device – 1 piece; 2) power supply – 1 pc.; 3) power cable – 1 pc.; 4) instruction manual combined with passport – 1 pc.; 5) bracket Ø10 mm. for attaching the device to a tripod – 1 PC.; 6) hex key 3 mm. - 1 PC.

Catalytic reforming is used to produce high-octane components of automobile gasoline, flavored concentrate for the production of individual aromatic hydrocarbons, as well as technical water. Isomerization of paraffin hydrocarbons is used to increase the octane number of C5 - C6 oil fractions by converting paraffins of normal structure into their isomers having a higher octane number.oroda. Hydrotreating of distillates is used to improve the quality and stability of light distillates, raw materials of catalytic cracking, as a result of the use of reactions of destructive hydrogenation of organosulfur compounds and hydrogenation of unsaturated hydrocarbons. Catalytic cracking is used to obtain additional amounts of light petroleum products, namely high-octane gasoline and diesel fuel, by decomposition of heavy oil fractions in the presence of a catalyst. Alkylation of isobutane with olefins is used to produce gasoline fractions with high stability and detonation resistance using the reaction of interaction of isobutane with olefins in the presence of a catalyst. Polymerization (oligomerization) of olefins is used to produce low molecular weight polymers (oligomers) of propylene and butylene used as motor fuel or raw materials for petrochemical synthesis. Hydrocracking is used to obtain an additional amount of light petroleum products by catalytic decomposition of heavy raw materials in the presence of hydrogen. Thermal cracking and Visbreaking is used to obtain in the mode of thermal cracking – additional amounts of light petroleum products by thermal decomposition of residues from oil distillation, in the mode of visbreaking – improving the quality of boiler fuel Coking is used to produce petroleum coke and an additional amount of light petroleum products from heavy residues. The raw materials are tar, thermal cracking residue, heavy gas oil. The products are, for example, petroleum coke.

The Meta-chrome digital gas flow meter is designed to maintain a given pressure and the ratio of the amount of gases (in the flow mode) or gas flow (in the intake mode) in vacuum installations with automatic and manual control. technical specifications The number of control channels is 2 (or more on request). The maximum flow rate for each of the channels is 700 cm3/min. The possibility of using gas correction coefficients, the most commonly used gases are listed in the leaker database. The accuracy of maintaining a given proportion of gases is 5%. The accuracy of maintaining the specified gas flow rates is 3%. Input pressures from 1 to 4 atm. Electric power supply from a single—phase AC network with voltage from 187 to 242 V, frequency (50 ± 1) Hz, operating mode - continuous. Power consumption (without a personal computer), no more than — 30 VA. Overall dimensions (width × depth × height), no more than 165×350×215 mm. Weight, not more than 5.5 kg.

NT-MDT Spectrum Instruments is an INTEGRA Nano IR–scattering scanning near‑field optical microscope (s-NSOM) designed for the infrared spectral range. The AFM probe is located in the focus of an optical system that directs the IR laser radiation to the sample and collects the optical response. The collected radiation is sent to the Michelson interferometer for optical analysis. The far-field component of the collected signal is suppressed by synchronous detection. The INTEGRA Nano IR system allows detecting the amplitude and phase of the near-field signal. The spatial resolution of the resulting reflection and absorption contrasts is approximately 10 nm and is determined only by the size of the tip of the probe.

Specialized wavelength-dispersive XRF analyzer based on the Cochois scheme is designed for high-precision determination of chemical elements U, Th, Mo, Au, W, Tl, As, Pb as well as other elements in ores, rocks and when developing the technogenic fields. Possibility to determine groups of elements without readjustment of crystal-analyzer. Exceptionally high resolution of the Koshua X-ray optical scheme with crystal-analyzer quartz 1011. Developed mathematical support. Principle of analyzer operation is based on the excitation of the fluorescent radiation of sample atoms being under examination by radiation coming from an X-ray tube. Spectrum decomposition of the fluorescence radiation is performed according to Cauchois method. The fluorescence radiation focused by analyzing crystal and standard line are marked on Rowland focal circle. Then, they are recorded by X-ray radiation detector in turn. The intensity of the fluorescent irradiation with a particular wavelength is directly proportional to the chemical element concentration in the material under examination.