PC-1 Portable compressor

The separation of some substances (the classic case is the separation of oxygen and argon) requires negative temperatures of the thermostat of chromatographic columns. technical specifications The lower temperature limit of the thermostat of columns with a cooling device based on an air conditioner is minus 5 °C. The error in maintaining the temperature of the thermostat of columns with a cooling device based on an air conditioner is + 0.05 °C. The power consumption of the cooling device based on an air conditioner, no more than — 640 VA. Overall dimensions of the cooling device based on the air conditioner, (width × depth × height), no more than — 620×480× 410 mm. The weight of the cooling device based on the air conditioner, no more than 32 kg. The lower limit of the temperature of the thermostat of columns with a liquid nitrogen cryoclap is minus 100 °C. The error of maintaining the temperature of the thermostat of columns with a liquid nitrogen cryoclave (in the temperature range less than 25 °C) + 0.1 °C. The power consumption of a cooling device with a liquid nitrogen cryoclave, no more than — 10 VA. Consumption of liquid nitrogen, not more than 0.1 l/h.

The dispenser "DAZH 4000" is designed for automatic insertion of liquid samples into the evaporator of the gas chromatograph, provides: control from the software, setting variable parameters of algorithms for washing and sample entry, storing the operating parameters of the dispenser in the method. Technical characteristics: The number of vials in the carousel, pcs up to 30 The volume of installed vials, ml 0.1-2ml Number of injections from one vial 1-99 Replaceable syringes in volume, ml 10, 100, 250, 500 The volume of the injected sample, ml : from 0.01 to 500 The discreteness of setting the sample volume, µl: from 0.01 to 1 Sampling and insertion rate, µl/s: from 0.01 to 5000 The speed of needle insertion into the evaporator, discret 3 Immersion depth in the vial and evaporator, variable up to the length of the syringe needle, mm 1 – 99 The discreteness of the dive depth setting, mm 0,1 The number of pumping during sampling 0-15 Number of solvent washes 0-15 Needle exposure time in the evaporator, sec 0-99 The discreteness of setting the needle shutter speed, sec 1,0 Sample input modes Simple insertion, Sandwich, Solvent sandwich, Sandwich with internal standard Flushing mode From the vial Supply voltage, V (frequency, Hz) 220 (50) Power consumption, W 154 Weight, kg, no more 2,9 Overall dimensions, mm 175x270x420 Communication with the computer Ethernet

The gas chromatograph "Kristallux-4000M" is fully automated, starting from sample input and ending with chromatographic information processing, including the functions of automatic temperature control of thermostats, flow rates and pressure of the carrier gas (EUPG system), auxiliary gases, automatic ignition of detectors, flame burning control during operation, measurement of detector signals using Gorenje 24-bit ADC. Technical specifications: The detection limit of PID is 1,1x10-12 gS/s for h-hydrocarbons 1,1x10-12 gS/s for propane. The detection limit of DTP1.7x10-14 g/s for lindane 3.9x10`15 g/s for lindane (micro-ED) The detection limit of EZD1x10`13 grus for phosphorus in metaphos 8x10`13 g5/s for sulfur in metaphos or hydrogen sulfide PFD detection limit 1.5x10`14 g/s for phosphorus in metaphos 3x10`13 GM/s for nitrogen in azobenzene Detection limit of TID2x10`10 g/ml by hydrogen The detection limit of TcD is 5x10`13 g/s for benzene The detection limit of the FEED is 3x10`13 g/s for carbon in methane 3x10`13 g/s for carbon in methane Detection limit GID500:1 (M7-801) with the introduction of 1x10`12 g / ml of octafluoroaphthalene The signal-to-noise ratio of MSD 1500:1 (Maestro-oMS) when entering 1x10`12 g / ml of octafluoroaphthalene Linear dynamic range of PID x1*107 Linear dynamic range DTP1*108 The volume of the column thermostat is 14 (19)l The temperature of the column Current.Wednesday +3 °C to +400 °C (by special order up to 450 °C) (by special order from -10°C with use. cold. ust-ki)(by special order from -100 °C. with use. liquid, no.) The discreteness of the temperature setting is 0, ° C Temperature stability 0.01 °C Temperature programming speed 0t 0.1 to 125 °C/min (by special order up to 150 °C/min) The number of isotherms is not less than 30 The cooling rate of the column thermostat is from 400 to 50 °C3.3 min. The maximum temperature of the detector and evaporator is 450 °C Carrier gas consumption from 0 to 100 ml/min.(by special order up to 500 ml/min.) Carrier gas pressure (for capillary column) from 0 to 0.40 Mpa (by special order up to 1 MPa) The maximum inlet gas pressure on a special order is 0.5 MPA 1.25 MPA Hydrogen consumption 0-500 Air consumption 0-1000 Overall dimensions (width x depth x height) 550%500*500 mm Weight 39 kg Electric power supply from AC mains voltage (220.2) V, frequency (50 +1) Hz The maximum power consumption (in steady-state mode) is 900 VA.

Technical characteristics: DETECTOR - TYPE OF CHROMATOGRAPH - DETECTION LIMIT, G/S (G/ML) -STANDARD DEVIATION, % - LEVEL OF FLUCTUATIONAL NOISES, A (V) -DRIFT, А/H (V/H) FID Crystall-2000 5×10⁻¹² 2 2×10⁻¹⁴ 4×10 ⁻¹³ TCD Crystall-2000 (5×10⁻⁹) 2 (2×10⁻⁷) (2×10⁻⁵) ADC Crystall-2000 5×10⁻¹⁴ 4 1×10⁻¹² 8×10⁻¹¹ FPD-Р Crystall-2000 2×10⁻¹² 6 2×10⁻¹¹ 4×10⁻¹⁰ FPD-S Crystall-2000 2×10⁻¹¹ 10 2×10⁻¹¹ 4×10⁻¹⁰

The equilibrium steam dispenser "DRP-10 (DRP-13)" is designed for the introduction of volatile components from matrices into the chromatograph, the introduction of which into the chromatograph is impossible or undesirable. Examples of such matrices are natural, drinking and waste water, soil, biological fluids, food and beverages, various polymers, building materials, pharmaceutical products, etc. The use of DRP-10 (DRP-13) makes it possible to avoid contamination of the evaporator, column and chromatograph detector with non-volatile or non-volatile substances, to avoid the consumption of solvent required for extraction, to increase the reproducibility of analyses. Technical specifications The temperature of the thermostat of containers with a breakdown is from ambient temperature to 150 °C. The error of maintaining the temperature is not more than 0.1 ° C. The volume of the container with the sample is 20 ml, it is possible to use vials from 6 to 40 ml. The number of simultaneously thermostatically controlled containers is 4. The dosed volume of the equilibrium vapor is up to 2 ml. The temperature of the syringe is from ambient temperature to 150 °C. The gas consumption for purging is from 5 to 300 ml/min. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Overall dimensions (width × depth × height) — 350×270×170 mm. Power consumption — no more than 360 VA. Weight — no more than 6.5 kg.

It can be used as a primary source of carrier gas, since it is equipped with an additional gas purification system. This device is especially relevant when, for some reason, helium is not available to the consumer (for example, when working with a thermal conductivity detector - an accident). Due to the high thermal conductivity of hydrogen, TTP operates with significantly greater sensitivity than helium.

The flow regulator consists of the following parts: Body. It includes a connector for connection to the control controller and fittings for connecting the input and output gas lines. Calorimetric converter. Due to the heating of the gas along the flow section, the temperature difference is determined. The actuator (solenoid valve). The control board. A system of elements responsible for converting the signals that the user submits. TECHNICAL CHARACTERISTICS OF RD The gas pressure at the inlet is (0.4 + 0.04) MPa. Ranges of working gas flow rates — from 5 to 800 ml/min. The ability to specify the type of gas (nitrogen, helium, hydrogen, argon, air). Pressure ranges — from 0.001 to 0.40 MPa with a discreteness of 0.0001 MPa. The deviation of the carrier gas flow rate from the average value is + 1.5% in the flow range from 50 to 100 ml/min and + 0.5 ml/min in the flow range from 3 to 50 ml/min. Relative deviation of the average steady-state gas flow rate from the set value in the range from 3 to 100 ml/min: + 2.5%, but not less than 0.5 ml/min; from 100 to 200 ml/min.: + 5%; from 200 to 800 ml/min.: + 10%. The gas pressure at the inlet is (0.4 + 0.04) MPa. The deviation of the regulated output pressure of the regulator from the set value is not more than 1%.

The PA-1 single-channel portable aspirator is based on the PC-1 portable compressor. It provides air aspiration with a flow rate from 0.1 to 0.8 l/min. The aspirator is powered by an integral battery.

The autosampler is used to automate the process of entering samples of liquid consistency into chromatographs of the line "Kristallux", "Crystal", series "Color", LHM. The autosampler is compact in size and easy to operate. The device is compatible with different models of chromatographs and is suitable for many studies. When the device is working with the Crystallux series chromatographs, the autosampler can be controlled using the chromatographic equipment software, while no additional programs are required.

To determine small concentrations of substances, in some cases it is impossible to do without their concentration in special traps. An example of the need for such concentration is the determination of impurities in permanent gases (Ne, He, H2, Ar, O2, N2, Kr, Xe), the concentration of impurities is less than 1 ppm. Considering that these impurities can be not only hydrocarbons, but also permanent gases themselves, the use of direct detection of impurities by a catarometer is impossible. It is also not always possible to use highly sensitive but expensive detectors (GID, EDD, etc.). TECHNICAL CHARACTERISTICS The volume of the trap is 5 ml. The volume of the Dewar vessel (serial metal thermos) is 1200 ml. The concentration temperature range is from minus 88.6 (ethane) to minus 269 °C (helium). The ability to calibrate the chromatograph from the cylinder without disturbing the gas circuit. The possibility, simultaneously with concentration, to purify the gas intended for purging the trap from impurities (in a similar trap). Overall dimensions, no more than — 290 ×470 × 615 mm. Weight, not more than — 8 kg.

To analyze small concentrations of carbon monoxide (CO) and carbon dioxide (CO2), instead of the usual catarometer for these gases, a more sensitive PID is used, while carbon oxides are converted into methane (CH4) using reaction chromatography. The device implementing the conversion reaction is called a methanator, i.e. a device with a special catalyst that converts CO, CO2 into methane in a hydrogen current, while the latter is either a carrier gas itself, or is blown together with the carrier gas into the methanator through a tee. The methanator provides a highly efficient conversion reaction, while the detection limit of carbon oxides reaches 0.1 ppm. technical specifications Metanation temperature — 330 °C The coefficient of metanation is not less than 95 % The effective volume of the methanator is 1 ml.

The pyrolytic gas chromatography method is widely used in the study of polymer materials, plastics, rubbers, rubbers, paints and other high-molecular compounds of natural and artificial origin. The method is based on thermal decomposition of sample samples in an inert medium (without oxygen access), followed by chromatographic separation and analysis of the formed volatile compounds. Thus, the resulting pyrogram allows us to judge the composition of the original sample. Pyrolysis is also used in geochemical studies. Technical specifications The volume of the capsule is 56 ml. Pyrolysis temperature — from 200 to 1000 °C. The error of maintaining the temperature is not more than 1.0 ° C. The heating time of the sample to the pyrolysis temperature is no more than 2 seconds. The cooling time of the capsule when moving from the hot zone to the cold zone after pyrolysis is no more than 10 seconds. The time of continuous operation in the pyrolysis mode is no more than 60 seconds. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Power consumption — no more than 100 VA. Overall dimensions of the control unit (width ×depth×height) — 210×190×100 mm. Overall dimensions of the input node (width× depth×height) — 90×135×160 mm. The weight of the control unit is not more than 2.5 kg. The weight of the input node is not more than 0.9 kg.

Implements a thermogravimetric (air-thermal) method for determining the mass fraction of moisture, based on measuring the mass of the sample of the analyzed substance before and after drying, followed by calculating the values of the mass fraction of moisture. Air-thermal measuring installations ASESH-8 are registered in the State Register of Measuring Instruments under No. 58526-14, have a certificate of approval of the type of measuring instruments OC.C.31.005 And No. 56847.The installations undergo initial verification and have the appropriate certificate. General characteristics: - The presence of two independent drying chambers. - Possibility of simultaneous determination of humidity of 12 samples: Each drying chamber of the installation consists of 6 independent cells. You can put 2 buckets in each cell. Total capacity of the ASES Installation-8-2 – 24 bucs. - Convenient access to the cells of the drying chamber: On the front side of the cabinet there are four doors for access to the cells. - Natural ventilation: The absence of rotating elements ensures absolute noiselessness of operation and a long service life. - Built-in timer: The ASESH-8-2 installation has 4 timers, by means of which the end of the drying process is monitored in each section with the output of an audible signal and a light indication. - The output to the operating mode is 30 minutes: The power of air-thermal installations is 1200 watts. When entering the operating mode, the power consumption is the same as that of similar cabinets with low power. SCOPE OF DELIVERY : 1. Installation of ASESH-8-2 2. AO-3 cooler 3. Auxiliary accessories 4. Air-heat control unit: 5. Interface unit for connecting a personal computer with a scale (available on request); 6. software for processing and archiving measurements of humidity determination data; The program allows you to: Set the operating temperature in the chambers via a personal computer Set the necessary parameters of the sample drying process according to the selected method Display all current processes (predrying, drying, cooling) and parameters (temperature, time) during the tests. To monitor the process by means of an electronic timer with the output of an audible signal. Record all weighing results. Perform humidity calculations in accordance with standardized methods. To calculate the humidity with pre-drying, the program uses formulas that allow you to get an accurate result. Archive and print test results. According to the test results of FSUE "UNIIM", it is recommended to use a laboratory mill of the BLIZZARD series for sample preparation. SCOPE OF APPLICATION: 1. Crop production, agriculture and forestry. 2. Products of meat, dairy, fish, flour-milling, feed and microbiological industries. 3. Food industry products. 4. Cellulose, paper, cardboard and products made from them. 5. Medicines, chemical and pharmaceutical products and medical products. 6. Building materials. 7. Products of the logging and sawmilling and woodworking industry. 8. Ground, soils, mineral fertilizers. Technical specifications: The measurement range of the mass fraction of moisture, % from 0.5 to 80 Operating temperature range, °C from 45 to 160 The error of setting and maintaining the temperature in the working area, ° C, not more than 2.0 Limits of permissible absolute error, % ± 0.5 Power consumption, V• A, not more than 1200 Overall dimensions, mm 240 × 260 × 640 Overall dimensions of the cell, mm 75 x 40 x 165 (depth) Weight, kg 28.4

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), mixing of the contents of the syringe with oil is used to accelerate the extraction of gases (to achieve an equilibrium distribution of gases dissolved in oil between the liquid and gas phases). For this purpose, as well as automation of the mixing process, a special autonomous device for achieving equilibrium is produced. technical specifications The rotation speed of the syringe drum is 30 rpm./min. The rotation time (determined by the internal timer, after pressing the "Start" button) is 10 minutes. The number of syringes placed is 4. The volume of syringes is 20 or 50 ml. Power consumption, no more than — 14 VA. Overall dimensions, no more than 210×280×270 mm. Weight, not more than — 5 kg.

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), it is necessary to first fill a syringe with transformer oil with a carrier gas, and then, after achieving an equilibrium distribution of gases dissolved in oil between the liquid and gas phases, introduce the gas phase into the chromatograph (blow out the doses of the chromatograph dispenser tap). Moreover, the operations of filling the syringe and entering the sample are performed without air access. When filling the syringe, it is possible to fix the syringe stem at a certain volume. technical specifications The volume of syringes is 20 or 50 ml. The pressure at the outlet of the syringe filling line with argon is 0.5 atm. The range of ratios of volumes of the gas phase and oil (Vg/Vm) is from 0 to 1.5.

The gas distribution panel (hereinafter referred to as the panel) is designed to connect gas nodes and blocks of various analytical instruments, including chromatographs to shop gas lines. technical specifications Inlet pressure, not more than 0.8 MPa. The output pressure is from 0 to 0.4 MPa. Gas flow rate through each channel, not less than — 1000 cm3/min.