Laboratory mercury analyzer "RA-915Lab"

The gas distribution panel (hereinafter referred to as the panel) is designed to connect gas nodes and blocks of various analytical instruments, including chromatographs to shop gas lines. technical specifications Inlet pressure, not more than 0.8 MPa. The output pressure is from 0 to 0.4 MPa. Gas flow rate through each channel, not less than — 1000 cm3/min.

The liquid chromatograph "Lumachrom-M" provides maximum automation of the analysis. The device is controlled using specialized software, which in combination with the continuous eluent supply mode and the autosampler gives the maximum level of autonomy of operation. In addition, such a solution minimizes labor costs and the influence of the human factor. The unique design solutions of the chromatograph provide continuous pulsation-free flow of the mobile phase in both isocratic and gradient modes, as well as the ability to work with any column sizes. Thanks to the improved technical characteristics on the Lumachrom-M device, it is possible to implement a wider list of techniques and GOST compared to previous models.

Technical specifications: Method of ionization Plasma pulsed glow discharge Discharge gas Argon, consumption less than 1 l/hour Time-of-flight Mass Analyzer with mesh-free ion mirror Resolution 4000 The number of simultaneously defined components is unlimited Mass range 1-1000 m/z Detection limits 1-100 ppb Layer-by-layer resolution Up to 5 nm Depth of analysis Up to 30 microns The time for one analysis of a solid sample is 30 minutes (with the option of a revolver system – 3-5 minutes) Vacuum system 1 Booster pump and 2 TMN (240 l/sec) Overall dimensions 1450×780×1550 mm

The autosampler is used to automate the process of entering samples of liquid consistency into chromatographs of the line "Kristallux", "Crystal", series "Color", LHM. The autosampler is compact in size and easy to operate. The device is compatible with different models of chromatographs and is suitable for many studies. When the device is working with the Crystallux series chromatographs, the autosampler can be controlled using the chromatographic equipment software, while no additional programs are required.

Technical specifications: The upper limit of the measurement range is 5 mg/kg Analysis time 1-5 min Permissible sample weights are 10-500 mg The weight of the console is 17 kg Air pumping speed 1-3 l/min Dimensions and weight of the analyzer 470x210x110 mm; 7.5 kg Power supply of the PIRO-915+ 220 V, 700 W Analyzer power supply 220 V, 15 W Dimensions of the power supply and pumping unit no more than 400x280x135 mm The dimensions of the thermal camera unit and the remote optical unit are no more than 430x340x135 mm The upper limit of the measurement range for sample weighting is 20 mg 200 mg/kg

To determine small concentrations of substances, in some cases it is impossible to do without their concentration in special traps. An example of the need for such concentration is the determination of impurities in permanent gases (Ne, He, H2, Ar, O2, N2, Kr, Xe), the concentration of impurities is less than 1 ppm. Considering that these impurities can be not only hydrocarbons, but also permanent gases themselves, the use of direct detection of impurities by a catarometer is impossible. It is also not always possible to use highly sensitive but expensive detectors (GID, EDD, etc.). TECHNICAL CHARACTERISTICS The volume of the trap is 5 ml. The volume of the Dewar vessel (serial metal thermos) is 1200 ml. The concentration temperature range is from minus 88.6 (ethane) to minus 269 °C (helium). The ability to calibrate the chromatograph from the cylinder without disturbing the gas circuit. The possibility, simultaneously with concentration, to purify the gas intended for purging the trap from impurities (in a similar trap). Overall dimensions, no more than — 290 ×470 × 615 mm. Weight, not more than — 8 kg.

Technical characteristics: The set-top box is powered by AC (220 ± 22) V, 50 Hz Power consumption, VA, no more than 35 Continuous operation time, h 8 Overall dimensions: (LxWxH), mm, no more than 320x290x160 The weight of the console, kg, not more than 6.5 Air consumption, dm3/min 2 ... 5

Technical specifications: Operating spectral range, nm from 190 to 360 Limits of permissible absolute error of wavelength setting, nm ± 5 Detection limit of anthracene (wavelength 252 nm), ng/cm3, no more than 1 The limit of the permissible value of the relative mean square deviation of the output signal (n =5), % of the retention time over the peak area of 1.5 2 Limits of the permissible value of the relative change in the output signal (peak area) for 4 hours of continuous operation, % ± 5 Overall dimensions (LxWxH), mm, no more: 270x420x190 Weight, kg, not more than 9.5 Power consumption, V· A, not more than 50

The separation of some substances (the classic case is the separation of oxygen and argon) requires negative temperatures of the thermostat of chromatographic columns. technical specifications The lower temperature limit of the thermostat of columns with a cooling device based on an air conditioner is minus 5 °C. The error in maintaining the temperature of the thermostat of columns with a cooling device based on an air conditioner is + 0.05 °C. The power consumption of the cooling device based on an air conditioner, no more than — 640 VA. Overall dimensions of the cooling device based on the air conditioner, (width × depth × height), no more than — 620×480× 410 mm. The weight of the cooling device based on the air conditioner, no more than 32 kg. The lower limit of the temperature of the thermostat of columns with a liquid nitrogen cryoclap is minus 100 °C. The error of maintaining the temperature of the thermostat of columns with a liquid nitrogen cryoclave (in the temperature range less than 25 °C) + 0.1 °C. The power consumption of a cooling device with a liquid nitrogen cryoclave, no more than — 10 VA. Consumption of liquid nitrogen, not more than 0.1 l/h.

Technical specifications: Continuous operation time 8 hours Analyzer dimensions (LxWxH), mm, no more than 470x110x220 mm Overall dimensions of the pumping unit: (LxWxH), mm, no more than 360x110x125 mm Analyzer weight 7 kg The weight of the console is 7 kg Power supply 100 - 240 V Powered by an autonomous RA source-915+ - 6/14 In Powered by an autonomous source RP-91 - 12 V Power consumption 20 W Current frequency 50/60 Hz The mass of the pumping unit is 3 kg Average service life, years, at least 5 Volume of the injected sample, cm3 0.5 - 10.0 Air flow, dm3/min 0.8 - 4.2

The device is designed to extract target organic substances from liquid and solid samples. Implements the latest method of sample preparation in chemical analysis - extraction freezing with centrifugation of EVCB (Patents of the Russian Federation RU2303476/2007, RU2564999/2015, Patent of the Kyrgyz Republic KG388/2020, International Application PCT/RU2015/000615). Scope of application - hydrochemistry, chemical and toxicological analysis, biochemistry, food research, etc. technical specifications The temperature range of extraction freezing with centrifugation is from -(minus) 28 to +25 °C. Rotor speed with the possibility of programming the mode 100-8000 rpm Separation factor up to 6600 g Cryoextractor power supply from AC 220 V, 50 Hz Power consumption, not more than 0.3 kW The mass of the cryoextractor is not more than 50 kg Overall dimensions (HxWxD), mmxmmxmm no more than 900x600x600 Number of simultaneously extracted samples (individually on request)

Technical specifications: Continuous operation time 8 hours The dimensions of the analyzer are 470x220x110 mm The dimensions of the console are 340x240x120 mm Analyzer weight 7.5 kg The weight of the console is 5.5 kg Power supply 220 V Supply voltage of RA-915M: (220 ±22) V, 50 Hz URP supply voltage: (220±22) V, 50 Hz Power consumption of RA-915M: 35 VA URP power consumption: 220 VA Current frequency 50 Hz

The pyrolytic gas chromatography method is widely used in the study of polymer materials, plastics, rubbers, rubbers, paints and other high-molecular compounds of natural and artificial origin. The method is based on thermal decomposition of sample samples in an inert medium (without oxygen access), followed by chromatographic separation and analysis of the formed volatile compounds. Thus, the resulting pyrogram allows us to judge the composition of the original sample. Pyrolysis is also used in geochemical studies. Technical specifications The volume of the capsule is 56 ml. Pyrolysis temperature — from 200 to 1000 °C. The error of maintaining the temperature is not more than 1.0 ° C. The heating time of the sample to the pyrolysis temperature is no more than 2 seconds. The cooling time of the capsule when moving from the hot zone to the cold zone after pyrolysis is no more than 10 seconds. The time of continuous operation in the pyrolysis mode is no more than 60 seconds. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Power consumption — no more than 100 VA. Overall dimensions of the control unit (width ×depth×height) — 210×190×100 mm. Overall dimensions of the input node (width× depth×height) — 90×135×160 mm. The weight of the control unit is not more than 2.5 kg. The weight of the input node is not more than 0.9 kg.

To analyze small concentrations of carbon monoxide (CO) and carbon dioxide (CO2), instead of the usual catarometer for these gases, a more sensitive PID is used, while carbon oxides are converted into methane (CH4) using reaction chromatography. The device implementing the conversion reaction is called a methanator, i.e. a device with a special catalyst that converts CO, CO2 into methane in a hydrogen current, while the latter is either a carrier gas itself, or is blown together with the carrier gas into the methanator through a tee. The methanator provides a highly efficient conversion reaction, while the detection limit of carbon oxides reaches 0.1 ppm. technical specifications Metanation temperature — 330 °C The coefficient of metanation is not less than 95 % The effective volume of the methanator is 1 ml.

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), mixing of the contents of the syringe with oil is used to accelerate the extraction of gases (to achieve an equilibrium distribution of gases dissolved in oil between the liquid and gas phases). For this purpose, as well as automation of the mixing process, a special autonomous device for achieving equilibrium is produced. technical specifications The rotation speed of the syringe drum is 30 rpm./min. The rotation time (determined by the internal timer, after pressing the "Start" button) is 10 minutes. The number of syringes placed is 4. The volume of syringes is 20 or 50 ml. Power consumption, no more than — 14 VA. Overall dimensions, no more than 210×280×270 mm. Weight, not more than — 5 kg.

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), it is necessary to first fill a syringe with transformer oil with a carrier gas, and then, after achieving an equilibrium distribution of gases dissolved in oil between the liquid and gas phases, introduce the gas phase into the chromatograph (blow out the doses of the chromatograph dispenser tap). Moreover, the operations of filling the syringe and entering the sample are performed without air access. When filling the syringe, it is possible to fix the syringe stem at a certain volume. technical specifications The volume of syringes is 20 or 50 ml. The pressure at the outlet of the syringe filling line with argon is 0.5 atm. The range of ratios of volumes of the gas phase and oil (Vg/Vm) is from 0 to 1.5.