Photoionization (PID)

GC and MS interface Capillary direct interface, independent temperature control (50-300 0 S) The filament of the cathode (filament) is a double filament for electron ionization (EI), the maximum current is 300 µA. Double thread increases the service life. Two independent switchable cathodes Temperature of the ion radiation source Independent heating and temperature control, maximum value 350 0 C (adjustable) Transparent polymer window on the front panel there is no visual control of the state of the cathodes Ion radiation source Lenses made of ceramic and with a patented coating enhance the focusing effect, which significantly increases the efficiency of ionization, an electrode with a patented reflective surface improves focusing Tubular lenses enhance the focusing effect, which significantly increases the ionization efficiency, an electrode with a patented reflective surface improves focusing Energy ionization 10-100 eV The mass analyzer is a high-precision quadrupole with a filter that reduces the contamination of the main quadrupole and eliminates the influence of photonic noise on the analysis High-precision molybdenum quadrupole with prequadrupole (replaceable), which reduces the contamination of the main The detector is an electronic multiplier with a high-voltage secondary emiting electrode (dinode) of high energy 3D geometry to improve sensitivity. The amplifier of weak voltage signals effectively reduces network noise, improves the signal-to-noise ratio during electron ionization and provides a large linear dynamic range. It is possible to install an additional detector Mass range 2.0-1200 a.e.m. 1.5-1050 a.e.m. Mass stability Less than 0.1 a.e.m. for 48 hours Signal ratio noise At least 1500:1 with mass to charge (m/z) 272 At least 150:1 with mass to charge (m/z) 272 (with signal filtering 500:1) Linearity Not less than 107 Not less than 106 Precision < 5% RSD 9n=7, SIM, 100 fg OFN) no System sensitivity IDL < 10 fg (SIM mode, OFN according to m/z 272) no Maximum scanning speed 20000 a.m./s 11000 a.m./s Operating modes Scap, SIM, Scan/SIM, MicroScan and the innovative Flexible-SIM algorithm for finding trace amounts of components no Setting Automatic setting MSD on the PFTBA spectrum and m/z control of oxygen, nitrogen and water no Pumping pump Oil plate-rotor vacuum pump with a pumping speed of 66 l/min Oil plate-rotor vacuum pump with a pumping speed of 165 l/min Turbo pump Turbo molecular pump with magnetic levitation, with a pumping speed of 85 l/s (can be replaced by 300 l/s) Turbo molecular pump with magnetic levitation, with a pumping speed of 71 l/s (possible replacement by 260 l/s) RF detector power Allows you to use three points for calibration in the entire mass range and get good linearity in scanning mode Software Rus./ Eng. The ability to search and extract structural, graphical formulas. Library of 240,000 spectra. The ability to isolate individual components from overlapping peaks. In addition to spectra and compounds, the library contains the element name, formula, molecule structure, molecular weight, CAS number, analysis conditions, synonyms, and estimated or measured retention readings. The NIST EI library contains: drugs, metabolites and poisons, pesticides and fungicides, organic substances present in soil, water and air, amino acids, di- and tripeptides, common sample pollutants, common analytical derivatives, etc. Ethernet interface, remote access function implemented Touch screen Display of parameters and monitoring of system status no Built -in power supply Allows you to turn off the detector in normal mode if there is no power supply violation

Selective detector for organochlorine compounds and other halogens. It is also sensitive to compounds containing oxygen, phosphorus or aromatic rings, but to a lesser extent. Paraffins and simple hydrocarbons almost do not capture electrons and are not registered. The selectivity to hydrocarbons is 108. It is available in two versions — conventional EDD and micro-EDD, mainly for capillary columns (the second version is characterized by increased sensitivity). The level of fluctuation noise is up to 300 MV, the maximum signal is up to 5 V, the design of the ECD allows the use of argon, helium, and hydrogen as a carrier gas, in addition to nitrogen. Technical characteristic: 4.0*10-15 g/s for lindane

It operates in the mode of a helium ionization detector (GID) and is considered the most sensitive device for determining permanent gases. In addition, it is able to work in the EDD mode. Technical characteristic: 2.0*10`13 g/s by. methane or hydrogen

A feature of the POWDIX 600 X-ray diffractometer scheme is the vertical Bragg-Brentano optical scheme with a fixed horizontal sample position, which makes working with powdery materials, gels and other viscous substances more practical and convenient. The high detector resolution and precise positioning of the POWDIX 600 X-ray goniometer achieve an accuracy better than +/- 0.02° (2θ) over the entire angular range. In the POWDIX 600 diffractometer, the X-ray tube is cooled by an integrated closed water circuit, which can be serviced by any laboratory employee. A wide variety of sample holders (holder for massive samples, holder with rotation, phoneless cuvettes) expands the functionality of the POWDIX 600 and makes it an invaluable tool for scientific research in solid-state physics, materials science, chemistry, geology and other fields of science The diffractometer is included in the Russian State Register of Measuring Instruments.

It is used to determine hydrogen, oxygen, CO and combustible hydrocarbon gases, and its sensitivity to these compounds is higher than the sensitivity of an accident. The most widespread TCD was obtained for the analysis of hydrogen and oxygen, tk. its sensitivity to them is almost an order of magnitude higher than that of an accident. The principle of operation is based on fixing the thermal effect of catalytic combustion of the sample on the surface of the platinum filament. Technical characteristic: 1.8*10`10 g/ml of hydrogen

Selective detector for phosphorus and organosulphide compounds. It is used mainly for the analysis of sulfur-containing substances (hydrogen sulfide, mercaptans, thiophenes, etc.). The sensitivity for sulfur reaches 0.1. ppm. In addition, PFD has sufficient sensitivity and selectivity to compounds containing nitrogen, boron, tin, chromium, selenium, germanium, as well as CO, POPS, MgOx, $02, Ma, NOT C52. The selectivity of 5-containing compounds to hydrocarbons is 105. Technical characteristic: 8,0*10-13 g5/s by sulfur 1.0*10`13 g/s for phosphorus

Selective detector for organophosphorus and nitrogen compounds. It is also sensitive to compounds containing C, Az, but to a lesser extent. The sensitivity depends on the number of heteroatoms in the molecule. Selectivity to hydrocarbons is 104 for nitrogen, and 105 for phosphorus Technical characteristic: 2.0*10-13 m/s nitrogen 1.5*10`14 g/s for phosphorus

The most common, universal detector that is suitable for the analysis of a wide range of organic compounds. The sensitivity depends mainly on the number of carbon atoms. In combination with a methanator, it allows the analysis of carbon oxides at the level of 0.1 Rt. The level of fluctuation noise is up to 50 MV, the maximum signal is up to 2500 V. Technical characteristic: 1.2*10712 gs/s for hydrocarbons

The most versatile detector with two sensitive elements and automatic protection against their burnout. DTP has a significantly lower sensitivity compared to PID, but it is indispensable for determining permanent gases (helium, hydrogen, oxygen, nitrogen, argon, etc.). A distinctive feature is the extended dynamic range, in fact from 20 MV to 20 V and full automation of measurement, including current setting, compensation of the initial zero offset, switching measurement limits. It is available in several modifications, both in terms of volume and execution of sensitive elements. 'The level of fluctuation noise is up to 20 MV, the maximum signal is up to 20 V. Technical characteristics: 4.010710 g/ml of propane or teptan, 4.0 *10`10 g/ml of hydrogen