NPO Spektron

The X-ray fluorescence spectrometer SPECTROSCAN MAX-GF1(2)E-C combines two methods of detecting an analytical signal: diffraction on a crystal (wave dispersion - WDX) and energy dispersion (EDX) method, as well as sample delivery adapted for the analysis of large-size images. The collimation of the primary radiation of the X-ray tube and the special design of the sample presentation make it possible to analyze the sample over an area of 1 cm2 in 1 mm increments, and thus investigate the distribution of elements over an area. The spectrometer is designed to determine the contents of elements in the range from Ca to U in substances in solid, powdery, dissolved states, as well as deposited on the surface or deposited on filters. With the help of fixed energy dispersion channels, any one or two additional elements in the range from magnesium (Mg) to calcium (Ca) can be determined. With the help of this modification of the spectrometer, forensic and customs examinations, judicial and forensic medical examinations, as well as art-historical examinations are carried out.

The spectrometer is designed to determine the contents of elements in the range from Na to U in substances in solid, powdery, dissolved states, as well as deposited on the surface or deposited on filters. The principle of operation of the X-ray spectrometer is based on irradiation of the sample with primary radiation from an X-ray tube, measurement of the intensity of secondary fluorescent radiation from the sample at wavelengths corresponding to the elements to be determined, and subsequent calculation of the mass fraction of these elements according to a pre-constructed calibration characteristic, which is the dependence of the content of the element to be determined on the measured intensity. Secondary fluorescent radiation is decomposed into a spectrum using a crystal analyzer. Due to this, the X-ray fluorescence spectrometer has a high resolution, and therefore the ability to accurately analyze complex multicomponent substances.

The device is developed on the basis of the analyzer SPECTROSCAN SW-D3, allows you to determine the mass fraction of organochlorine compounds in oil according to GOST R 52247-2004 (method B) and GOST 33342-2015 (method B), the sulfur content in automotive fuel, oil and liquid petroleum products in accordance with GOST R 52660-2006 / GOST ISO 20884-2016 and GOST R 53203-2008 / GOST 33194-2014, as well as to determine the mass fraction of chlorine and sulfur in any liquid samples in accordance with standardized techniques (methods). Implements arbitration methods for determining the mass fraction of organochlorine compounds in oil and the sulfur content in automobile fuel. The analyzer has successfully passed the interlaboratory tests under the guidance of JSC "VNII NP" (TK31). As a result of the tests, the accuracy of the method for determining the mass fraction of organochlorine compounds using the SPECTROSCAN CLSW analyzer was found to comply with the requirements of GOST R 52247-2004, method B, and the accuracy of the method was determined in the range of the mass fraction of organochlorine compounds from 1 ppm to 50 ppm. Determination of the mass fraction of organochlorine compounds in oil involves sampling of oil, distillation of naphtha fraction (204 ° C), washing of naphtha from hydrogen sulfide and inorganic chlorides. An internal standard is introduced into naphtha extracted from oil – a solution of bismuth in a non-polar solvent and an analysis is carried out. When determining the sulfur content, the analysis is carried out without additional sample preparation. The analyzer is a proprietary development of NPO "SPEKTRON". The device is manufactured in St. Petersburg mainly from domestic components. There is a conclusion of the Ministry of Industry and Trade on the production of products in the territory of the Russian Federation. The operator's actions when performing measurements are minimized: - the number/name of the sample is entered from the built-in keyboard; - the sample is poured into two cuvettes; - the obtained samples are placed in the analyzer and measurements are started. The analyzer performs all subsequent actions automatically without operator involvement: - calculates and displays the chlorine and/or sulfur content in the sample; - calculates convergence - the difference in determining the mass fraction of an element in the first and second samples; - prints measurement results on the built-in printer.

Technical Regulation TR CU 013/2011 "On requirements for automotive and aviation gasoline, diesel and marine fuel, jet fuel and fuel oil" imposes requirements for the content of sulfur and metals in automotive fuel. The analyzer allows you to measure, in order to confirm the conformity of the fuel, according to the following indicators: mass fraction of sulfur, concentration of iron, manganese and lead. The analyzer implements an arbitration method for measuring the mass fraction of sulfur in automotive fuel of the third, fourth and fifth classes according to GOST R 52660-2006 / GOST ISO 20884-2016, and also allows you to measure the mass fraction of iron, manganese and lead. The MSW SPECTROSCOPE is designed taking into account the requirements for measuring low sulfur and metal contents in petroleum products. Meets the requirements for equipment and precision standards: GOST R 52660-2006 / GOST ISO 20884-2016, GOST R 53203-2008, GOST 33194-2014, ASTM D6334. The design of the analyzer allows it to be used in mobile laboratories. The operator's actions when performing measurements are minimized: - the number/name of the sample is entered from the built-in keyboard; - the sample is poured into two cuvettes; - the obtained samples are placed in the analyzer and measurements are started. The analyzer performs all subsequent actions automatically without operator involvement: - calculates and displays the content of elements in the sample; - calculates convergence - the difference in determining the content of elements in the first and second samples; - prints measurement results on the built-in printer.

The analyzer is designed to determine the mass fraction of sulfur in automotive fuel in accordance with GOST R 52660-2006 / GOST ISO 20884-2016, ASTM D6334, as well as in oil and petroleum products according to GOST R 53203-2008 / GOST 33194-2014, ASTM D2622, GB/T 11140-2008. Depending on the customer's needs, the analyzer is configured to work in accordance with a particular standard. Implements an arbitration method for measuring the mass fraction of sulfur in automobile fuel of the third, fourth and fifth classes. The device is designed specifically for high-quality and fast X-ray fluorescence analysis of fuel in accordance with the technical regulations "On requirements for automotive and aviation gasoline, diesel and marine fuel, jet fuel and heating oil", which establishes an arbitration X-ray fluorescence wave dispersion method for determining the mass fraction of sulfur in automotive fuels of the third, fourth and fifth classes. The wave dispersion sulfur analyzer SPECTROSCAN SW-D3 is designed taking into account all the requirements for the process of X-ray fluorescence elemental analysis of low sulfur contents in petroleum products. The operator's actions when performing measurements are minimized: - the number/name of the sample is entered from the built-in keyboard; - the sample is poured into two cuvettes; - the obtained samples are placed in the analyzer and measurements are started. The analyzer performs all subsequent actions automatically without operator involvement: - calculates and displays the sulfur content in the sample; - calculates convergence - the difference in determining the mass fraction of sulfur in the first and second samples; - prints measurement results on the built-in printer.

The IS-T and IS X-ray absorption flow SPECTROSCAN analyzers for sulfur in oil are designed to determine the mass fraction of sulfur in the flow of oil/petroleum products in the range from 0.02% to 6.00% (IS-T) or 0.04% to 6.0% (IS). Analyzers can be used for technological control during transportation and storage of oil, as well as during mixing (compounding) operations. The design of the analyzers allows them to be placed both independently and as part of a unit for measuring oil quality indicators (BIC) or a system for measuring the quantity and quality of oil (CIC). They are available in explosion-proof version. The analyzers have the function of automatically accounting for the influence of the density of the analyzed medium, as well as the content of water and chloride salts in it on the result of determining the mass fraction of sulfur. Structurally, the analyzers are a complete product of high factory readiness, having a block-modular design and including all the necessary functional devices to ensure efficient and safe operation.

The spectrometer is designed to determine the contents of elements in the range from Ca to U in substances in solid, powdery, dissolved states, as well as deposited on the surface or deposited on filters. The principle of operation of the spectrometer is based on irradiation of the sample with primary radiation from an X-ray tube, measurement of the intensity of secondary fluorescent radiation from the sample at wavelengths corresponding to the elements being determined, and subsequent calculation of the mass fraction of these elements according to a pre-constructed calibration characteristic, which is the dependence of the content of the element being determined on the measured intensity. Secondary fluorescent radiation is decomposed into a spectrum using a crystal analyzer. Due to this, the spectrometer has a high resolution, and therefore the ability to accurately analyze complex multicomponent substances.

The analyzer is designed to determine the mass fraction of sulfur from 3 million-1 (ppm) in oil and petroleum products in accordance with GOST R 51947-2002, GOST 32139-2019, GOST R EN ISO 20847-2010 / GOST ISO 20847-2014, ASTM D4294, GB/T 17040-2019. Implements an arbitration method for measuring the mass fraction of sulfur for oil, automotive fuels of class K2, K3, jet engine fuel, aviation gasoline, fuel oil and marine fuel, and is also used for operational control of sulfur content in automotive fuels of Class 4 and 5, gas oils, bitumen, lubricating oils and their components and other petroleum products. The analyzer greatly simplifies the routine analysis procedure. Intuitive interface provides convenience and ease of use. The analyzer is a proprietary development of NPO "SPEKTRON". The device is manufactured in St. Petersburg mainly from domestic components. Minimum operator actions: - calibration is selected and the name of the sample is entered; - two cuvettes are filled with a sample; - the obtained samples are placed in the analyzer and measurements are started; - all subsequent actions are performed automatically: - the average value of the mass fraction of sulfur is calculated and displayed; - repeatability is calculated; - the results are checked for compliance with the selected standard; - measurement results are printed on the built-in printer and saved.

The analyzer is designed to determine the mass fraction of sulfur in automotive fuel in accordance with GOST R 52660-2006 / GOST ISO 20884-2016, ASTM D6334, as well as in oil and petroleum products according to GOST R 53203-2008 / GOST 33194-2014, ASTM D2622, GB/T 11140-2008. Depending on the customer's needs, the analyzer is configured to work in accordance with a particular standard. Implements an arbitration method for measuring the mass fraction of sulfur in automobile fuel of the third, fourth and fifth classes. The device is designed specifically for high-quality and fast X-ray fluorescence analysis of fuel in accordance with the technical regulations "On requirements for automotive and aviation gasoline, diesel and marine fuel, jet fuel and heating oil", which establishes an arbitration X-ray fluorescence wave dispersion method for determining the mass fraction of sulfur in automotive fuels of the third, fourth and fifth classes. The wave dispersion sulfur analyzer SPECTROSCAN SW-D3 is designed taking into account all the requirements for the process of X-ray fluorescence elemental analysis of low sulfur contents in petroleum products. The operator's actions when performing measurements are minimized: - the number/name of the sample is entered from the built-in keyboard; - the sample is poured into two cuvettes; - the obtained samples are placed in the analyzer and measurements are started. The analyzer performs all subsequent actions automatically without operator involvement: - calculates and displays the sulfur content in the sample; - calculates convergence - the difference in determining the mass fraction of sulfur in the first and second samples; - prints measurement results on the built-in printer.

The analyzer allows you to determine the content of sulfur and nitrogen in oil and petroleum products (diesel fuel, gasoline, kerosene, gas oil and any distillate petroleum products), hydrocarbon gas, liquefied petroleum gas (LPG), natural gas, liquefied natural gas (LNG), chemical synthesis products, biological materials by ultraviolet fluorescence and chemiluminescence. The analyzer is a proprietary development of NPO "SPEKTRON". The device is manufactured in St. Petersburg mainly from domestic components. There is a conclusion of the Ministry of Industry and Trade on the production of products in the territory of the Russian Federation. The analyzer is designed to determine: - mass fraction of sulfur in accordance with GOST ISO 20846-2016, GOST 34712-2021, GOST R 56866-2016, GOST 34237-2017, ASTM D5453-19, ASTM D6667-21, ASTM D7551-15, ISO 20729-17 ; - the mass fraction of nitrogen in accordance with ASTM D4629-17. A wide range of concentrations: from ultra-low to high. Modular principle: Each detector is a separate module. The device is equipped individually for each specific task. The possibility of simultaneous determination of sulfur and nitrogen in the analysis process. The principle of operation of the analyzer is to burn the test sample in an oxygen-enriched atmosphere or air at a temperature of 1050 ° C. The sulfur dioxide (SO2) and nitrogen oxide (NO) formed during combustion are transferred by carrier gas to the detection units with preliminary removal of water vapor, on the desiccant, and soot, on the filter. Determination of sulfur is carried out by ultraviolet fluorescence. Determination of nitrogen by chemiluminescence.