Chromatographic columns for HPLC

Partially universal detector. It is used for the analysis of most organic compounds, including aromatic and aliphatic (except methane) hydrocarbons, heterocyclic compounds, phenols, phthalates, pesticides, amines, ketones, aldehydes, esters, mercaptans. It does not register compounds whose ionization threshold is higher than 10.2 eV (for example, acetonitrile, methanol). Technical characteristic: 5.0*10`13 g/s for benzene

It is used to determine hydrogen, oxygen, CO and combustible hydrocarbon gases, and its sensitivity to these compounds is higher than the sensitivity of an accident. The most widespread TCD was obtained for the analysis of hydrogen and oxygen, tk. its sensitivity to them is almost an order of magnitude higher than that of an accident. The principle of operation is based on fixing the thermal effect of catalytic combustion of the sample on the surface of the platinum filament. Technical characteristic: 1.8*10`10 g/ml of hydrogen

Selective detector for organophosphorus and nitrogen compounds. It is also sensitive to compounds containing C, Az, but to a lesser extent. The sensitivity depends on the number of heteroatoms in the molecule. Selectivity to hydrocarbons is 104 for nitrogen, and 105 for phosphorus Technical characteristic: 2.0*10-13 m/s nitrogen 1.5*10`14 g/s for phosphorus

Selective detector for organochlorine compounds and other halogens. It is also sensitive to compounds containing oxygen, phosphorus or aromatic rings, but to a lesser extent. Paraffins and simple hydrocarbons almost do not capture electrons and are not registered. The selectivity to hydrocarbons is 108. It is available in two versions — conventional EDD and micro-EDD, mainly for capillary columns (the second version is characterized by increased sensitivity). The level of fluctuation noise is up to 300 MV, the maximum signal is up to 5 V, the design of the ECD allows the use of argon, helium, and hydrogen as a carrier gas, in addition to nitrogen. Technical characteristic: 4.0*10-15 g/s for lindane

TDS-2 is a syringe (see Fig. 1), which is installed on the evaporator of the chromatograph. The device is equipped with a crane that cuts off the carrier gas line when removing the rod with the sorption tube from the thermal desorber. When the tap is open, the stem is lowered to the lower position and the sorption tube is inserted into the evaporator brought to the desired temperature. In the conditions of the upper position of the rod, it is also possible to displace air by purging the sorption tube with a carrier gas. Technical characteristics of TDS-2 The heating time to the desorption temperature is no more than 1 sec. The cooling time when moving to a cold zone is no more than 10 seconds. Outer diameter 5-0.1 mm Dimensions of the sorbent chamber: diameter 3.4+0.3 mm length 52 mm (470 µl) Volume (for solid samples) 90 µl Operating temperature ranges* from 50° to 400 °C Overall dimensions (height with the rod fully extended) 320 mm. Weight 0.325 kg.

Selective detector for phosphorus and organosulphide compounds. It is used mainly for the analysis of sulfur-containing substances (hydrogen sulfide, mercaptans, thiophenes, etc.). The sensitivity for sulfur reaches 0.1. ppm. In addition, PFD has sufficient sensitivity and selectivity to compounds containing nitrogen, boron, tin, chromium, selenium, germanium, as well as CO, POPS, MgOx, $02, Ma, NOT C52. The selectivity of 5-containing compounds to hydrocarbons is 105. Technical characteristic: 8,0*10-13 g5/s by sulfur 1.0*10`13 g/s for phosphorus

The metering valve for the introduction of gas samples is designed for the introduction of gas under excessive pressure into the chromatograph. Cranes differ in the number of moves (4, 6, 8, 10, 12) and have two provisions "Selection" — "Analysis". In addition to dosing, cranes can be used to switch chromatographic columns, elements of gas circuits, etc. The tap can be installed either on the side panel of the chromatograph, or directly into the analytical module instead of, or together with the evaporator of the chromatograph, while it is used as a back-purge tap or for hot sample entry. Additionally, the tap for hot entry can be equipped with heated pipelines. technical specifications The dose volume is from 0.25 to 5.0 ml (at the request of the consumer, the dose volume can be increased to 10 ml and reduced to 0.1 ml). The maximum temperature of the tap is no more than 160 °C. The pressure in the crane line is not more than 0.48 MPa. The angle of rotation of the crane handle — depending on the number of strokes.

The composition of the TDS-4 includes the thermal desorber itself (the thermostat of the sorption tube, a cryolovushka, an automatic switching valve, a touch control panel), a heated transition line that is installed in the evaporator\ Technical characteristics of TDS-4 Temperature of thermal desorption, 0C to 400 The heating rate of the sorption tube, 0C/min up to 500 Trap temperature, 0C from minus 25 to 400 Trap heating speed, 0C to 2000 The method of heating the trap is direct Tap heating temperature, 0C to 250 Transition line heating temperature, 0C to 250 Continuous operation mode Dimensions of the sorption tube, (diameter; length), mm. Material glass, stainless steel 5/114 (on request 6/115, 6,3/89 and their combinations) Tube material glass or stainless steel (SS316) Method of trap cooling without using liquid refrigerant The number of regulated gas flows is not less than 2 There is an automatic leak test function There is a function of automatic purging of the sorption tube Electric power supply from 187 to 242 V, 50 Hz Power consumption, W not more than 700

The reverse purge valve is a 4-way valve designed to change the direction of the flow of the eluent through the nozzle column and blow off heavy components from the beginning of the column in the opposite direction into the detector. The crane is attached to the bottom panel (bottom) of the module, while taking the temperature of the column thermostat. The two upper fittings (see Fig.) are used to connect the column, the other two are connected to the evaporator and the detector.

The metering valve for the analysis of liquefied gas (KDSG) is designed for the introduction of liquefied gas or other liquid under excessive pressure into the evaporator of the chromatograph. KDSG is a 4-way crane, in which a dose of a certain volume is installed. The tap is installed on the evaporator of the chromatograph. A dose of any volume can be installed on the tap. Dose change can be performed by the operator. The amount of the dose volume is indicated on the tag. Technical specifications The dose volume is from 0.25 to 4.0 µl (at the request of the consumer, the dose volume can be increased up to 10 µl). The tap temperature is no more than 150 °C. The pressure in the crane line is not more than 0.48 MPa. The angle of rotation of the crane handle is 90 °C.

To switch the nozzle columns, conventional taps (reverse purge, 6-, 8- and 10-port) are used, which, however, are not suitable for switching capillary columns. An alternative way to switch capillary columns is to change the flows in the capillary columns, which is produced by the so-called "Dins switches" (PD). TECHNICAL CHARACTERISTICS of PD The switching time setting range is from 0.1 to 999 min. Switching time is 0.1 s. The dead volume of the crane is less than 1 µl. The temperature of the tap is no more than 350 °C. The pressure in the crane line is not more than 0.4 MPa. Electric power supply — 5 V.

The TDS-3 includes a heating column with a sorption tube, which is installed on the evaporator of the chromatograph and a control unit located on a special bracket on the right side panel of the chromatograph Technical characteristics of TDS-3 Desorption temperature (column heating), 0C to 400 Heating speed, 0C/min at least 500 The cooling time when moving to a cold zone is no more than 10 seconds. Cooling time from 300 0C to 50 0C, min. no more than 10 Continuous operation mode Power consumption, W not more than 250 Dimensions of the sorption tube, (Ø, length), mm. Material glass, stainless steel 5/110, 5/114, 6/115, 6.35/89 Electric power supply from 187 to 242 V, 50 Hz. The display of the measured temperature and the setting of the temperature on the display is The discreteness of setting the desorption temperature, 0C 0.1

Device for dosing of liquefied gases is made for insertion of liquids and liquefied gases under the pressure of 7 MPa into the chromatograph. Injection of liquefied gas without de-gassing is provided by cooling of valve, and it greatly reduces inaccuracy of the analysis results. Cooling temperature is set by temperature regulator. Visual control of absence of de-gassing and flow control of the analyzed fluid is provided. Dose volume is form 0.2 to 2 mcl. Valve of VICI production or dispenser valve of our own production is used directly as a sample-valve.

They are used for sampling natural and liquefied gas. In the company "Meta-chrome" you can buy the following gas samplers: PGO-50M; PGO-400; BDP 12-2-9,8 (aluminum, subcompact); PU. The PGO-50 M, PGO-400 and PU models are used to take samples of liquefied hydrocarbon gases that are affected by the overpressure of stationary tanks and or their own vapors. Sampling is carried out according to GOST 14921-78. The BTP 12-2-9.8 device is used for sampling, storing and transporting samples of gases that are under pressure. The device is made of aluminum and is designed for a small liter. Sampling is carried out according to GOST 31370-2008. INDICATOR BDP7 BDP7 BDP12 BDP12 BDP16 PGO-400 PGO-50M Volume, l. 0,7 1 2 4 10 0,4 0,05 Outer diameter, mm 70 70 120 120 160 50 35 Length, mm 360 480 368 593 800 400 325 Working pressure, MPa 9.8 5.0 9.0 The number of refills up to the operating pressure, times at least 5000 Case material AMg6M 12X18

When determining the total gas content (air) and humidity of transformer oil, direct injection of transformer oil into the evaporator of the chromatograph is used. The sample volume is up to 25 µl, the evaporator temperature is 250-350 °C. The main problem with such an input is the protection of the chromatographic column from transformer oil. For this purpose, a special evaporator is used with the possibility of oil accumulation at the bottom of the evaporator and its subsequent discharge, and a replaceable pre-column that protects the column from oil residues that have passed the evaporator. technical specifications The volume of the evaporator is 10 ml. The number of replaceable pre—columns in the device kit is 5. The temperature of the evaporator is from 250 to 350 °C. The possibility of draining the transformer oil accumulated in the evaporator.