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The reverse purge valve is a 4-way valve designed to change the direction of the flow of the eluent through the nozzle column and blow off heavy components from the beginning of the column in the opposite direction into the detector. The crane is attached to the bottom panel (bottom) of the module, while taking the temperature of the column thermostat. The two upper fittings (see Fig.) are used to connect the column, the other two are connected to the evaporator and the detector.

The flow regulator consists of the following parts: Body. It includes a connector for connection to the control controller and fittings for connecting the input and output gas lines. Calorimetric converter. Due to the heating of the gas along the flow section, the temperature difference is determined. The actuator (solenoid valve). The control board. A system of elements responsible for converting the signals that the user submits. TECHNICAL CHARACTERISTICS OF RD The gas pressure at the inlet is (0.4 + 0.04) MPa. Ranges of working gas flow rates — from 5 to 800 ml/min. The ability to specify the type of gas (nitrogen, helium, hydrogen, argon, air). Pressure ranges — from 0.001 to 0.40 MPa with a discreteness of 0.0001 MPa. The deviation of the carrier gas flow rate from the average value is + 1.5% in the flow range from 50 to 100 ml/min and + 0.5 ml/min in the flow range from 3 to 50 ml/min. Relative deviation of the average steady-state gas flow rate from the set value in the range from 3 to 100 ml/min: + 2.5%, but not less than 0.5 ml/min; from 100 to 200 ml/min.: + 5%; from 200 to 800 ml/min.: + 10%. The gas pressure at the inlet is (0.4 + 0.04) MPa. The deviation of the regulated output pressure of the regulator from the set value is not more than 1%.

A block of gas filters for lines with a pressure of up to 15 MPa. The volume, length, connection dimensions, type of connections with supply pipelines are specified when ordering.

When determining the total gas content (air) and humidity of transformer oil, direct injection of transformer oil into the evaporator of the chromatograph is used. The sample volume is up to 25 µl, the evaporator temperature is 250-350 °C. The main problem with such an input is the protection of the chromatographic column from transformer oil. For this purpose, a special evaporator is used with the possibility of oil accumulation at the bottom of the evaporator and its subsequent discharge, and a replaceable pre-column that protects the column from oil residues that have passed the evaporator. technical specifications The volume of the evaporator is 10 ml. The number of replaceable pre—columns in the device kit is 5. The temperature of the evaporator is from 250 to 350 °C. The possibility of draining the transformer oil accumulated in the evaporator.

It can be used as a primary source of carrier gas, since it is equipped with an additional gas purification system. This device is especially relevant when, for some reason, helium is not available to the consumer (for example, when working with a thermal conductivity detector - an accident). Due to the high thermal conductivity of hydrogen, TTP operates with significantly greater sensitivity than helium.

The device is designed to extract target organic substances from liquid and solid samples. Implements the latest method of sample preparation in chemical analysis - extraction freezing with centrifugation of EVCB (Patents of the Russian Federation RU2303476/2007, RU2564999/2015, Patent of the Kyrgyz Republic KG388/2020, International Application PCT/RU2015/000615). Scope of application - hydrochemistry, chemical and toxicological analysis, biochemistry, food research, etc. technical specifications The temperature range of extraction freezing with centrifugation is from -(minus) 28 to +25 °C. Rotor speed with the possibility of programming the mode 100-8000 rpm Separation factor up to 6600 g Cryoextractor power supply from AC 220 V, 50 Hz Power consumption, not more than 0.3 kW The mass of the cryoextractor is not more than 50 kg Overall dimensions (HxWxD), mmxmmxmm no more than 900x600x600 Number of simultaneously extracted samples (individually on request)

The pyrolytic gas chromatography method is widely used in the study of polymer materials, plastics, rubbers, rubbers, paints and other high-molecular compounds of natural and artificial origin. The method is based on thermal decomposition of sample samples in an inert medium (without oxygen access), followed by chromatographic separation and analysis of the formed volatile compounds. Thus, the resulting pyrogram allows us to judge the composition of the original sample. Pyrolysis is also used in geochemical studies. Technical specifications The volume of the capsule is 56 ml. Pyrolysis temperature — from 200 to 1000 °C. The error of maintaining the temperature is not more than 1.0 ° C. The heating time of the sample to the pyrolysis temperature is no more than 2 seconds. The cooling time of the capsule when moving from the hot zone to the cold zone after pyrolysis is no more than 10 seconds. The time of continuous operation in the pyrolysis mode is no more than 60 seconds. Electric power supply from the AC network with voltage (220index) V, frequency (50 ± 1) Hz. Power consumption — no more than 100 VA. Overall dimensions of the control unit (width ×depth×height) — 210×190×100 mm. Overall dimensions of the input node (width× depth×height) — 90×135×160 mm. The weight of the control unit is not more than 2.5 kg. The weight of the input node is not more than 0.9 kg.

The gas chromatograph "Kristallux-4000M" is fully automated, starting from sample input and ending with chromatographic information processing, including the functions of automatic temperature control of thermostats, flow rates and pressure of the carrier gas (EUPG system), auxiliary gases, automatic ignition of detectors, flame burning control during operation, measurement of detector signals using Gorenje 24-bit ADC. Technical specifications: The detection limit of PID is 1,1x10-12 gS/s for h-hydrocarbons 1,1x10-12 gS/s for propane. The detection limit of DTP1.7x10-14 g/s for lindane 3.9x10`15 g/s for lindane (micro-ED) The detection limit of EZD1x10`13 grus for phosphorus in metaphos 8x10`13 g5/s for sulfur in metaphos or hydrogen sulfide PFD detection limit 1.5x10`14 g/s for phosphorus in metaphos 3x10`13 GM/s for nitrogen in azobenzene Detection limit of TID2x10`10 g/ml by hydrogen The detection limit of TcD is 5x10`13 g/s for benzene The detection limit of the FEED is 3x10`13 g/s for carbon in methane 3x10`13 g/s for carbon in methane Detection limit GID500:1 (M7-801) with the introduction of 1x10`12 g / ml of octafluoroaphthalene The signal-to-noise ratio of MSD 1500:1 (Maestro-oMS) when entering 1x10`12 g / ml of octafluoroaphthalene Linear dynamic range of PID x1*107 Linear dynamic range DTP1*108 The volume of the column thermostat is 14 (19)l The temperature of the column Current.Wednesday +3 °C to +400 °C (by special order up to 450 °C) (by special order from -10°C with use. cold. ust-ki)(by special order from -100 °C. with use. liquid, no.) The discreteness of the temperature setting is 0, ° C Temperature stability 0.01 °C Temperature programming speed 0t 0.1 to 125 °C/min (by special order up to 150 °C/min) The number of isotherms is not less than 30 The cooling rate of the column thermostat is from 400 to 50 °C3.3 min. The maximum temperature of the detector and evaporator is 450 °C Carrier gas consumption from 0 to 100 ml/min.(by special order up to 500 ml/min.) Carrier gas pressure (for capillary column) from 0 to 0.40 Mpa (by special order up to 1 MPa) The maximum inlet gas pressure on a special order is 0.5 MPA 1.25 MPA Hydrogen consumption 0-500 Air consumption 0-1000 Overall dimensions (width x depth x height) 550%500*500 mm Weight 39 kg Electric power supply from AC mains voltage (220.2) V, frequency (50 +1) Hz The maximum power consumption (in steady-state mode) is 900 VA.

It operates in the mode of a helium ionization detector (GID) and is considered the most sensitive device for determining permanent gases. In addition, it is able to work in the EDD mode. Technical characteristic: 2.0*10`13 g/s by. methane or hydrogen

The autosampler is used to automate the process of entering samples of liquid consistency into chromatographs of the line "Kristallux", "Crystal", series "Color", LHM. The autosampler is compact in size and easy to operate. The device is compatible with different models of chromatographs and is suitable for many studies. When the device is working with the Crystallux series chromatographs, the autosampler can be controlled using the chromatographic equipment software, while no additional programs are required.

The principle of operation of the electronic diaphanoscope YANTAR is to assess the vitreousness of the image obtained using a digital camera. The vitreous value is calculated using a software-implemented algorithm using special calibration equations. The analysis time is 1 minute. Automation of the vitreous assessment avoids the error associated with the subjective opinion of a specialist. The use of specially developed calibration standards based on optical filters for uniform adjustment of diaphanoscopes permits to coordinate the operation of two or more devices remotely. The interlaboratory error in determining the vitreousness on the devices included in the network does not exceed the standard. All the results of the determination of the vitreousness of wheat with the corresponding grain images are stored in the archive. If necessary, specialists can print the protocols of the current or any of the previous definitions. THE ALGORITHM OF OPERATION: 1. Pour the grains into the cassette and close the lid made of transparent glass. 2. Install the cassette in the diaphanoscope. 3. Launch the program. 4. Choose a product 5. Software processing of the digital image of grains in accordance with the selected product 6. Calculation of computer results. In 2023, a new national standard GOST R "Wheat. Determination of vitreousness by optical-computer method".

The gas distribution panel (hereinafter referred to as the panel) is designed to connect gas nodes and blocks of various analytical instruments, including chromatographs to shop gas lines. technical specifications Inlet pressure, not more than 0.8 MPa. The output pressure is from 0 to 0.4 MPa. Gas flow rate through each channel, not less than — 1000 cm3/min.