Laboratory reactor 150 liters

Characteristics Maximum heating temperature, °C up to +200 °С Minimum cooling temperature -120 °C Speed range, rpm 60-600 Shaft diameter, mm 14 Nutrition 220 V Heater power, W 9000 (bath heating) Volume, l 150 Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating Engine power, W 90, 3:1 gear motor

The unit is designed for testing fresh catalysts, deactivated in laboratory conditions and equilibrium (used in industry). The volume of the loaded catalyst is from 5 to 12 grams, the loading of raw materials (vacuum gas oil) is 1-3 grams. Conradson coking capacity should not exceed 10%. After cracking, the degree of coking of the catalyst is determined directly at the installation. Liquid and gaseous cracking products are analyzed by three gas chromatographs with automatic dispensers, which makes it possible to determine the degree of conversion and selectivity of the catalyst.

Catalytic reforming is used to produce high-octane components of automobile gasoline, flavored concentrate for the production of individual aromatic hydrocarbons, as well as technical water. Isomerization of paraffin hydrocarbons is used to increase the octane number of C5 - C6 oil fractions by converting paraffins of normal structure into their isomers having a higher octane number.oroda. Hydrotreating of distillates is used to improve the quality and stability of light distillates, raw materials of catalytic cracking, as a result of the use of reactions of destructive hydrogenation of organosulfur compounds and hydrogenation of unsaturated hydrocarbons. Catalytic cracking is used to obtain additional amounts of light petroleum products, namely high-octane gasoline and diesel fuel, by decomposition of heavy oil fractions in the presence of a catalyst. Alkylation of isobutane with olefins is used to produce gasoline fractions with high stability and detonation resistance using the reaction of interaction of isobutane with olefins in the presence of a catalyst. Polymerization (oligomerization) of olefins is used to produce low molecular weight polymers (oligomers) of propylene and butylene used as motor fuel or raw materials for petrochemical synthesis. Hydrocracking is used to obtain an additional amount of light petroleum products by catalytic decomposition of heavy raw materials in the presence of hydrogen. Thermal cracking and Visbreaking is used to obtain in the mode of thermal cracking – additional amounts of light petroleum products by thermal decomposition of residues from oil distillation, in the mode of visbreaking – improving the quality of boiler fuel Coking is used to produce petroleum coke and an additional amount of light petroleum products from heavy residues. The raw materials are tar, thermal cracking residue, heavy gas oil. The products are, for example, petroleum coke.

The unit is designed to simulate and study the processes of delayed coking occurring at elevated temperature and pressure in a stainless steel reactor made in the form of a flask with a spherical bottom and a removable lid. The installation allows you to obtain experimental data, select and optimize the parameters of the technological process, test various variants of raw mixtures, determine the material balance of the process, the characteristics of the process products. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. The power supply is a single-phase AC network with a voltage of 230-240V 50-60 Hz. The average service life of the autoclave is 6 years. TECHNICAL CHARACTERISTICS Operating pressure range, MPa 0÷0.6 Reactor operating temperature range, 0C 50÷550 The discreteness of the temperature setting is 0C 1 Relative error of temperature maintenance, 0C ± 0.2 Reactor material steel 12x18N10T Power consumption, kW not more than 3 Overall dimensions (HxWxD) 1600x1100x495 Weight, kg 240 Continuous operation mode

Minimum cooling temperature -120 °C Speed range, rpm 60-1000 Nutrition 220 V Heater power, W 1500 (bath heating) Volume, l 3 Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating 7 mm Engine power, W 60 Maximum plate heating temperature, °C up to +200 °С

Characteristics Minimum cooling temperature -120 °C Speed range, rpm 60-600 Nutrition 220 V Heater power, W 3000 (bath heating) Volume, l 20 Vacuum, MPa 0.098 Material stirrer head: stainless steel coated with PTFE 12 mm Engine power, W 90, 3:1 gear motor Maximum plate heating temperature, °C up to +200 °С

Monophase gas (the phase state of reagents at room temperature is liquid or gas). Monophase liquid (the phase state of reagents at room temperature is liquid). Two-phase (gas-liquid heterophase system). Temperature: operating range 500C – 6000C, 8000C.(three-zone heating furnace). Pressure: operating range 0.1 – 60, 100, 200 MPA. In the photo: A universal bench laboratory installation for the study of basic organic synthesis processes in a reactor with a fixed catalyst layer The unit is designed (tested) for the study of a wide range of heterogeneous catalytic reactions, including: Hydrogenation processes in the gas phase. Hydrogenation processes in the liquid phase. Gas-phase dehydration of aliphatic and aromatic alcohols. Dehydration of aromatic alcohols in the liquid phase. Alkylation of aromatic hydrocarbons with olefins and alcohols. Hydroalkylation of aromatic compounds with ketones. Dehydrogenation of chemical compounds of various classes.

Characteristics Valve(s) material PTFE (Teflon). This is what the seals are made from. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum ≥-0.098 Nutrition 220 V/ 50 Hz Volume, l 5 Mixer power, W 90 Material glass Boro 3.3., photoroplast, steel SS304

The unit is designed to determine the so-called Davison index (the ratio of catalyst fractions with a particle size of less than 20 microns before and after analysis), which characterizes the abrasion resistance of microspherical catalysts of the cracking process in a fluidized bed. The installation is included in the register of testing facilities.

The laboratory unit is designed to evaluate the activity of heterogeneous catalysts in a reactor with a fixed bed for the hydrotreating process. Ambient temperature from +10 to +35C; The relative humidity of the air is not more than 80% at a temperature of 25C;. Single-phase AC network with a voltage of 220 V ± 10% with a frequency of 50 Hz The average service life of the installation is 5 years. TECHNICAL CHARACTERISTICS OF THE HYDROTREATING AND HYDROGENATION UNIT Reactor: 1 piece Reactor volume, 240 ml Material 12X18H10T Inner diameter, mm 24 Length, mm 500 Operating temperature range, 0C 20÷600 Operating pressure range, MPa 0÷10 Removable pocket for thermocouples,mm 600 Reactor furnace: 1 piece Type of furnace Type of furnace Casement Number of thermostatic zones, pcs 3 The length of the full heated zone of the furnace, mm 450 The length of each of the four thermostatic zones, mm 150 The length of the isothermal zone of the furnace, mm 300 The power consumed by each isothermal zone, W 800 Power consumed by all three zones of the furnace, W 2400 The discreteness of the temperature setting, 0C 1 Hydrogen flow rate shaper: 1 piece Type of shaper, RGE Bronkhost Range of supported expenses, l/h 0-100 Inlet pressure, 100 bar Nitrogen flow rate shaper: 1 piece The type of the shaper, the leak (Nat2) Hy-Lok Range of supported expenses, l/h 0-10 Inlet pressure, 0-100 bar Raw material consumption shaper: 1 piece Shaper type, liquid pump KAPPA 10 Supported flow range, ml/min 0-10 Output pressure, 0-400 bar Raw material capacity: 1 piece Volume, l 4 Maximum pressure, atm 4 Working pressure, atm 0.2-1 Raw Materials Oil Installation: 1 piece Operating cycle of the installation, h 120 Inlet gas pressure calculated H2, N2, MPa 10 Actuation pressure of mechanical safety valves, 9.9 MPa Supply voltage 220V 50Hz The power consumption of the entire installation is not more than, kW 3 Installation weight without cabinet, kg 120 Overall dimensions, mm 1800x865x550 Overall dimensions of the cabinet, mm 2000x800x880

The device consists of the following parts: 200 liter glass flask with jacket; Glass cover with five openings for connecting additional equipment/components; Top drive mixer with anchor; Drip funnel; Condenser with receiving vessel; Control block. All parts are mounted on a steel frame with wheels. Thanks to this, the reactor can be easily moved from one part of the room to another. It has a modular design, easy to assemble and disassemble. All connections are equipped with chemically resistant fluoroplastic gaskets. Glass accessories are made of durable 3.3 borosilicate glass. Characteristics Voltage, V 220 Reaction flask volume, l 200 Material stainless steel, borosilicate glass 3.3 Execution movable steel frame

Characteristics Valve(s) material PTFE (Teflon). The seals are also made from it. Rotation speed, rpm 60-1000 Motor operating principle asynchronous, brushless, AC Shaft diameter, mm 7 Vacuum 0.098 Nutrition 220 V/ 50 Hz Volume, l 1 Mixer power, W 40 Material Stirrer rod: SS304, PTFE coated blades Housing material and other glass elements - GG17 glass (3.3).

Characteristics Maximum heating temperature, °C up to +200 °С Minimum cooling temperature -120 °C Speed range, rpm 60-600 Shaft diameter, mm 12 Nutrition 220 V Heater power, W 4000 (bath heating) Volume, l thirty Vacuum, MPa 0.098 Material stirrer head: stainless steel with PTFE coating Engine power, W 90, 3:1 gear motor