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The gas distribution panel (hereinafter referred to as the panel) is designed to connect gas nodes and blocks of various analytical instruments, including chromatographs to shop gas lines. technical specifications Inlet pressure, not more than 0.8 MPa. The output pressure is from 0 to 0.4 MPa. Gas flow rate through each channel, not less than — 1000 cm3/min.

Device for dosing of liquefied gases is made for insertion of liquids and liquefied gases under the pressure of 7 MPa into the chromatograph. Injection of liquefied gas without de-gassing is provided by cooling of valve, and it greatly reduces inaccuracy of the analysis results. Cooling temperature is set by temperature regulator. Visual control of absence of de-gassing and flow control of the analyzed fluid is provided. Dose volume is form 0.2 to 2 mcl. Valve of VICI production or dispenser valve of our own production is used directly as a sample-valve.

MAES analyzers for recording atomic emission spectra with a time resolution of 1 ms are based on highly sensitive photodiodes and a special switching board for simultaneous reading of several sections of the spectra. The assembly of the rulers is installed on the "Grand" spectrometer. A " Flow" or twin-jet arc plasmatron is used to excite the atomic emission spectra of powder samples. The ATOM software registers the selected spectral lines and provides their processing according to the specified algorithms, taking into account the number and brightness of flashes (i.e. particle size). Recording the spectra of powder samples with a large time resolution makes it possible to estimate the number and size of individual particles, identify their composition and determine the concentrations of elements in each particle, promptly assess the uniformity of the distribution of certain elements to be determined and expand the possibilities of spectral analysis without significant changes in sample preparation. Main application areas: mass analysis of powder geological samples by scintillation to determine gold, silver, platinum group metals, iridium, rhodium, etc. with detection limits up to 0.01 g/t; qualitative determination of the composition of inclusions and mineral particles.

The separation of some substances (the classic case is the separation of oxygen and argon) requires negative temperatures of the thermostat of chromatographic columns. technical specifications The lower temperature limit of the thermostat of columns with a cooling device based on an air conditioner is minus 5 °C. The error in maintaining the temperature of the thermostat of columns with a cooling device based on an air conditioner is + 0.05 °C. The power consumption of the cooling device based on an air conditioner, no more than — 640 VA. Overall dimensions of the cooling device based on the air conditioner, (width × depth × height), no more than — 620×480× 410 mm. The weight of the cooling device based on the air conditioner, no more than 32 kg. The lower limit of the temperature of the thermostat of columns with a liquid nitrogen cryoclap is minus 100 °C. The error of maintaining the temperature of the thermostat of columns with a liquid nitrogen cryoclave (in the temperature range less than 25 °C) + 0.1 °C. The power consumption of a cooling device with a liquid nitrogen cryoclave, no more than — 10 VA. Consumption of liquid nitrogen, not more than 0.1 l/h.

The most common, universal detector that is suitable for the analysis of a wide range of organic compounds. The sensitivity depends mainly on the number of carbon atoms. In combination with a methanator, it allows the analysis of carbon oxides at the level of 0.1 Rt. The level of fluctuation noise is up to 50 MV, the maximum signal is up to 2500 V. Technical characteristic: 1.2*10712 gs/s for hydrocarbons

Liquid thermostats from Primelab are reliable and high-quality devices for maintaining and controlling liquid temperature in laboratory conditions. Models with different bath volumes (4 liters, 8 liters, 15 liters, 30 liters) allow you to choose the appropriate option depending on your needs and volume of work. The pump capacity is 15 liters per minute, which ensures efficient circulation of liquid in the bath. Digital/intelligent control allows you to easily and accurately set and maintain the desired temperature. The temperature control range from +20 to +200 degrees Celsius provides the ability to work with a wide range of substances and laboratory processes. Liquid thermostats from Primelab are the ideal solution for laboratories and scientific research, guaranteeing accuracy, reliability and ease of use.

The KOV-4 type air compressor is designed to supply flame detectors of gas chromatographs with air. Technical specifications: Capacity, at least, l/min 3 Outlet air pressure, 0.25+5 MPa% Pressure stability at constant flow rate, not more than 0.0007 MPa Engine power consumption, max, VA 100 Receiver volume, l 9 Noise level, no more, 60 dBa Weight, not more than, kg 19 Overall dimensions (width×depth×height), not more than, mm 235×755×440 Single-phase mains voltage 220 V, 50 Hz

The flow regulator consists of the following parts: Body. It includes a connector for connection to the control controller and fittings for connecting the input and output gas lines. Calorimetric converter. Due to the heating of the gas along the flow section, the temperature difference is determined. The actuator (solenoid valve). The control board. A system of elements responsible for converting the signals that the user submits. TECHNICAL CHARACTERISTICS OF RD The gas pressure at the inlet is (0.4 + 0.04) MPa. Ranges of working gas flow rates — from 5 to 800 ml/min. The ability to specify the type of gas (nitrogen, helium, hydrogen, argon, air). Pressure ranges — from 0.001 to 0.40 MPa with a discreteness of 0.0001 MPa. The deviation of the carrier gas flow rate from the average value is + 1.5% in the flow range from 50 to 100 ml/min and + 0.5 ml/min in the flow range from 3 to 50 ml/min. Relative deviation of the average steady-state gas flow rate from the set value in the range from 3 to 100 ml/min: + 2.5%, but not less than 0.5 ml/min; from 100 to 200 ml/min.: + 5%; from 200 to 800 ml/min.: + 10%. The gas pressure at the inlet is (0.4 + 0.04) MPa. The deviation of the regulated output pressure of the regulator from the set value is not more than 1%.

When analyzing gases dissolved in transformer oil using the ARP method (equilibrium vapor analysis), it is necessary to first fill a syringe with transformer oil with a carrier gas, and then, after achieving an equilibrium distribution of gases dissolved in oil between the liquid and gas phases, introduce the gas phase into the chromatograph (blow out the doses of the chromatograph dispenser tap). Moreover, the operations of filling the syringe and entering the sample are performed without air access. When filling the syringe, it is possible to fix the syringe stem at a certain volume. technical specifications The volume of syringes is 20 or 50 ml. The pressure at the outlet of the syringe filling line with argon is 0.5 atm. The range of ratios of volumes of the gas phase and oil (Vg/Vm) is from 0 to 1.5.

To determine small concentrations of substances, in some cases it is impossible to do without their concentration in special traps. An example of the need for such concentration is the determination of impurities in permanent gases (Ne, He, H2, Ar, O2, N2, Kr, Xe), the concentration of impurities is less than 1 ppm. Considering that these impurities can be not only hydrocarbons, but also permanent gases themselves, the use of direct detection of impurities by a catarometer is impossible. It is also not always possible to use highly sensitive but expensive detectors (GID, EDD, etc.). TECHNICAL CHARACTERISTICS The volume of the trap is 5 ml. The volume of the Dewar vessel (serial metal thermos) is 1200 ml. The concentration temperature range is from minus 88.6 (ethane) to minus 269 °C (helium). The ability to calibrate the chromatograph from the cylinder without disturbing the gas circuit. The possibility, simultaneously with concentration, to purify the gas intended for purging the trap from impurities (in a similar trap). Overall dimensions, no more than — 290 ×470 × 615 mm. Weight, not more than — 8 kg.

Partially universal detector. It is used for the analysis of most organic compounds, including aromatic and aliphatic (except methane) hydrocarbons, heterocyclic compounds, phenols, phthalates, pesticides, amines, ketones, aldehydes, esters, mercaptans. It does not register compounds whose ionization threshold is higher than 10.2 eV (for example, acetonitrile, methanol). Technical characteristic: 5.0*10`13 g/s for benzene

The metering valve for the introduction of gas samples is designed for the introduction of gas under excessive pressure into the chromatograph. Cranes differ in the number of moves (4, 6, 8, 10, 12) and have two provisions "Selection" — "Analysis". In addition to dosing, cranes can be used to switch chromatographic columns, elements of gas circuits, etc. The tap can be installed either on the side panel of the chromatograph, or directly into the analytical module instead of, or together with the evaporator of the chromatograph, while it is used as a back-purge tap or for hot sample entry. Additionally, the tap for hot entry can be equipped with heated pipelines. technical specifications The dose volume is from 0.25 to 5.0 ml (at the request of the consumer, the dose volume can be increased to 10 ml and reduced to 0.1 ml). The maximum temperature of the tap is no more than 160 °C. The pressure in the crane line is not more than 0.48 MPa. The angle of rotation of the crane handle — depending on the number of strokes.